STRUCTURAL CHARACTERIZATION OF THE BETA-SI3N4 WHISKER AL INTERFACES IN A BETA-SI3N4 WHISKER AL ALLOY-6061 COMPOSITE-MATERIAL

被引:24
作者
NING, XG [1 ]
PAN, J [1 ]
HU, KY [1 ]
YE, HQ [1 ]
机构
[1] CHANGSHA INST TECHNOL,CHANGSHA 410073,PEOPLES R CHINA
来源
PHILOSOPHICAL MAGAZINE A-PHYSICS OF CONDENSED MATTER STRUCTURE DEFECTS AND MECHANICAL PROPERTIES | 1992年 / 66卷 / 05期
关键词
D O I
10.1080/01418619208201591
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The structural characterization of the whisker matrix interface in a beta-Si3N4 whisker-Al alloy 6061 composite was investigated by high-resolution transmission electron microscopy (HRTEM). It was shown that there existed a nearly amorphous layer (2-3 nm thickness) between the whiskers and the Al matrix. Mg segregation at the whisker Al interface was revealed by energy-dispersive X-ray analysis. HRTEM observations indicated that MgO and MgAl2O4 nanocrystalline particles were easily formed at the whisker-Al interface in the composite owing to Mg segregation at the interface during the manufacturing of the composite. The Mg2Si particles (strengthening phase in the matrix) precipitated preferentially at the whisker-Al interface when the composite had been given a T6 heat treatment. Specific orientation relationships between the MgAl2O4 or Mg2Si particles and the beta-Si3N4 whiskers were found. The problems associated with characterizing the microstructure of a whisker-matrix interface in an Al alloy composite reinforced by whiskers are also discussed.
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页码:811 / 821
页数:11
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