SEPARATION AND DETERMINATION OF 5-HYDROXYMETHYL-2-FURALDEHYDE AND 2-FURALDEHYDE IN FRUIT JUICES BY MICELLAR ELECTROKINETIC CAPILLARY CHROMATOGRAPHY WITH DIRECT SAMPLE INJECTION

被引：21

作者：

CORRADINI, D

CORRADINI, C

机构：

[1] Istituto di Cromatografia, CNR, Area della Ricerca di Roma, 1-00016 Monterotondo Stazione, Rome

来源：

JOURNAL OF CHROMATOGRAPHY | 1992年 / 624卷 / 1-2期

关键词：

D O I：

10.1016/0021-9673(92)85700-4

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The separation of 5-hydroxymethyl-2-furaldehyde (5-HMF) and 2-furaldehyde (2-FA), which are recognized indices of deteriorative changes in some commercially processed foods, was investigated by micellar electrokinetic capillary chromatography (MECC), employing sodium dodecyl sulphate as the anionic surfactant. The effects of micellar concentration, temperature and the addition of methanol or acetonitrile on the migration times and selectivity were investigated. MECC was successfully applied to the determination of 5-HMF and 2-FA in grapefruit juice by an internal standard method without any sample pretreatment.

引用

页码：503 / 509

页数：7

共 28 条

[1] DETERMINATION OF SOME DRUGS BY MICELLAR ELECTROKINETIC CAPILLARY CHROMATOGRAPHY - THE PSEUDO-EFFECTIVE MOBILITY AS PARAMETER FOR SCREENING [J].