SAMPLE INTRODUCTION IN CORRELATION LIQUID-CHROMATOGRAPHY - APPLICATION, PROPERTIES AND WORKING-CONDITIONS FOR A NOVEL INJECTION SYSTEM

被引:26
作者
MARS, C [1 ]
SMIT, HC [1 ]
机构
[1] UNIV AMSTERDAM,ANALYT CHEM LAB,NIEUWE ACHTERGRACHT 166,1018 WV AMSTERDAM,NETHERLANDS
关键词
D O I
10.1016/S0003-2670(00)80496-1
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
To apply correlation liquid chromatography in practice, a reliable, accurate and simple injection system is essential. The injection system described is suitable. The system is tested thoroughly for different sample concentrations. The effects of possible non-idealities and incorrect working conditions are studied. The resulting disturbances are listed, so that inappropriate operating conditions can be traced and eliminated. To demonstrate the performance of the system, a standard mixture of polynuclear aromatic hydrocarbons is analysed and the results are compared with those obtained by conventional chromatography. The injection system and some special software greatly facilitates the practical use of correlation chromatography. © 1990.
引用
收藏
页码:193 / 208
页数:16
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