THE EFFECT OF SOME ADDITIVES ON THE STILLE PD0-CATALYZED CROSS-COUPLING REACTION

被引：90

作者：

GRONOWITZ, S

BJORK, P

MALM, J

HORNFELDT, AB

机构：

[1] Organic Chemistry 1, Chemical Center, University of Lund, 22100 Lund

来源：

JOURNAL OF ORGANOMETALLIC CHEMISTRY | 1993年 / 460卷 / 01期

关键词：

D O I：

10.1016/0022-328X(93)80368-L

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

It has been found that the addition of cupric oxide to the cross-coupling reaction (Stille reaction) of 2-tributylstannylpyridine with various halobenzenes and heterocyclic halides leads to a much faster reaction and higher yields. This is also the case for the formation of thieno[3,2-h]-1,6-naphthyridine from 2-(2-trimethylstannyl-3-pyridyl)-1,3-dioxolane and t-butyl-N-(2-bromo-3-thienyl)carbamate.

引用

页码：127 / 129

页数：3

共 17 条

[1] Basolo F., 1968, INORG SYNTH, V11, P108
[2] Coulson DR, 1971, INORG SYN, V13, P121, DOI DOI 10.1002/9780470132449.CH23
[3] SYNTHESIS OF THE 6 ISOMERIC THIENO[C]-FUSED 1,5-NAPHYTHYRIDINES AND 1,6-NAPHTHYRIDINES
GRONOWITZ, S
MALM, J
HORNFELDT, AB
[J]. COLLECTION OF CZECHOSLOVAK CHEMICAL COMMUNICATIONS, 1991, 56 (11A) : 2340 - 2351
[4] GRONOWITZ S, 1984, CHEM SCRIPTA, V24, P5
[5] GRONOWITZ S, 1960, ARK KEMI, V16, P309
[6] 3-STANNYLCYCLOBUTENEDIONES AS NUCLEOPHILIC CYCLOBUTENEDIONE EQUIVALENTS - SYNTHESIS OF SUBSTITUTED CYCLOBUTENEDIONES AND CYCLOBUTENEDIONE MONOACETALS AND THE BENEFICIAL EFFECT OF CATALYTIC COPPER IODIDE ON THE STILLE REACTION
LIEBESKIND, LS
FENGL, RW
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1990, 55 (19) : 5359 - 5364
[7] PALLADIUM-CATALYZED COUPLING OF HETEROARYL ALKYLSTANNANES WITH HETEROARYL HALIDES IN THE PRESENCE OF SILVER(I)OXIDE
MALM, J
BJORK, P
GRONOWITZ, S
HORNFELDT, AB
[J]. TETRAHEDRON LETTERS, 1992, 33 (16) : 2199 - 2202
[8] SYNTHESIS OF 5-CYCLOPROPYLURACIL AND 5-CYCLOPROPYLCYTOSINE BY THE PD(0)-CATALYZED COUPLING REACTION
PETERS, D
HORNFELDT, AB
GRONOWITZ, S
[J]. JOURNAL OF HETEROCYCLIC CHEMISTRY, 1991, 28 (06) : 1629 - 1631
[9] SYNTHESIS OF VARIOUS 5-ARYLSUBSTITUTED CYTOSINES
PETERS, D
HORNFELDT, AB
GRONOWITZ, S
[J]. JOURNAL OF HETEROCYCLIC CHEMISTRY, 1991, 28 (06) : 1613 - 1617
[10] SYNTHESIS OF VARIOUS 5-SUBSTITUTED URACILS
PETERS, D
HORNFELDT, AB
GRONOWITZ, S
[J]. JOURNAL OF HETEROCYCLIC CHEMISTRY, 1990, 27 (07) : 2165 - 2173

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