RAPID AND SIMPLE DETERMINATION OF AFLATOXIN-M1 IN MILK IN THE LOW PARTS PER 1012 RANGE

被引:24
作者
GAUCH, R
LEUENBERGER, U
BAUMGARTNER, E
机构
来源
JOURNAL OF CHROMATOGRAPHY | 1979年 / 178卷 / 02期
关键词
D O I
10.1016/S0021-9673(00)92513-5
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A method for extracting aflatoxin M1 [a carcinogen from Aspergillus flavus and A. parasiticus] from milk is proposed in which the use of disposable Extrelut clean-up columns simplifies the analysis considerably in comparison with existing methods. The quantitative determination is based on 1-dimensional TLC and fluorescence densitometric measurement. The detection limit is 5 ppt (parts per 1012) in milk and the recovery is 78 .+-. 4% at a level of 50 ppt.
引用
收藏
页码:543 / 549
页数:7
相关论文
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