MODIFIED SOL-GEL PROCESS FOR THE PRODUCTION OF LEAD TITANATE FILMS

被引：79

作者：

MILNE, SJ

PYKE, SH

机构：

[1] Division of Ceramics, School of Materials, University of Leeds, Leeds

来源：

JOURNAL OF THE AMERICAN CERAMIC SOCIETY | 1991年 / 74卷 / 06期

关键词：

LEAD TITANATE; SOL-GEL; FILMS; LIGANDS; PROCESSING;

D O I：

10.1111/j.1151-2916.1991.tb04120.x

中图分类号：

TQ174 [陶瓷工业]; TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

A modified sol-gel process has been developed for the production of thin films of PbTiO3. The new route uses the mixed ligand complex titanium diisopropoxide bis(acetylacetonate), Ti(OC3H7)2(CH3COCHCOCH3)2, in place of titanium tetraisopropoxide, Ti(OC3H7)4. For base-catalyzed conditions, the maximum thickness of crack-free PbTiO3 films after one high-temperature firing cycle is 1-mu-m. This value represents a twofold increase in thickness over that obtained using existing sol-gel routes based on Ti(OC3H7)4.

引用

页码：1407 / 1410

页数：4

共 12 条

[1] Bradley D. C., 1978, METAL ALKOXIDES
[2] Budd K., 1985, P BRIT CERAMIC SOC, V36, P107
[3] Budd K.D., 1986, MATER RES SOC S P, V73, P711
[4] BUDD KD, 1986, THESIS U ILLINOIS UR
[5] TRANSPARENT ZIRCONIA GEL-MONOLITH FROM ZIRCONIUM ALKOXIDE
DEBSIKDAR, JC
[J]. JOURNAL OF NON-CRYSTALLINE SOLIDS, 1986, 86 (1-2) : 231 - 240
[6] DOSCH RG, 1984, MATER RES SOC S P, V32, P157
[7] PREPARATION OF FERROELECTRIC PZT FILMS BY THERMAL-DECOMPOSITION OF ORGANOMETALLIC COMPOUNDS
FUKUSHIMA, J
KODAIRA, K
MATSUSHITA, T
[J]. JOURNAL OF MATERIALS SCIENCE, 1984, 19 (02) : 595 - 598
[8] FUKUSHIMA J, 1976, AM CERAM SOC BULL, V55, P1064
[9] Gurkovich S R, 1984, ULTRASTRUCTURE PROCE, P152
[10] LACOURSE WC, 1986, SCI CERAMIC CHEM PRO, P304

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