SYNTHESIS IN DRY MEDIA COUPLED WITH MICROWAVE IRRADIATION - APPLICATION TO THE PREPARATION OF ENAMINOKETONES

被引：136

作者：

RECHSTEINER, B ^{[1
]}

TEXIERBOULLET, F ^{[1
]}

HAMELIN, J ^{[1
]}

机构：

[1] UNIV RENNES 1,CNRS,PHYSICOCHIM STRUCT GRP 3,CAMPUS BEAULIEU,F-35042 RENNES,FRANCE

来源：

TETRAHEDRON LETTERS | 1993年 / 34卷 / 32期

关键词：

MICROWAVES; DRY MEDIA; ENAMINOKETONES; ACYLAMINES;

D O I：

10.1016/S0040-4039(00)60678-0

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Beta-diketones react with a variety of amines and aminoesters over clay K10 or silica under microwave irradiation in open vessels to give within a few minutes, the corresponding enaminoketones with good yields. According to the reaction conditions acylamines may also result.

引用

页码：5071 / 5074

页数：4