LIQUID-CHROMATOGRAPHY OF ORGANOTIN COMPOUNDS ON CYANOPROPYL SILICA-GEL

被引：23

作者：

PRAET, A

DEWAELE, C

VERDONCK, L

VANDERKELEN, GP

机构：

[1] STATE UNIV GHENT,ORGAN CHEM LAB,KRIJGSLAAN 281 S4,B-9000 GHENT,BELGIUM

[2] STATE UNIV GHENT,ALGEMENE & ANORGAN CHEM LAB,B-9000 GHENT,BELGIUM

来源：

JOURNAL OF CHROMATOGRAPHY | 1990年 / 507卷

关键词：

D O I：

10.1016/S0021-9673(01)84222-9

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Several stationary phases were evaluated for the liquid chromatography of organotin compounds. Cyanopropyl-derivatized silica gels are the most versatile phases for this type of analysis. In order to reduce stationary phase activity, an iodine chloride "on-column" pretreatment was developed. This leads to very fast quantitative and qualitative separations, as was demonstrated by the analysis of organotin standards, orgnotin-containing tungsten carbonyl complexes and organotin halides for reaction kinetic studies. © 1990.

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页码：427 / 437

页数：11

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