DETERMINATION OF 1,3-, 1,6-, 1,8-DINITROPYRENES AND 1-NITROPYRENE BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY WITH CHEMILUMINESCENCE DETECTION

被引：4

作者：

Hayakawa, Kazuichi ^{[1
]}

Miyazaki, Motoichi ^{[1
]}

机构：

[1] Kanazawa Univ, Fac Pharmaceut Sci, Kanazawa, Ishikawa 920, Japan

来源：

ANALYTICAL SCIENCES | 1991年 / 7卷

关键词：

dinitropyrene; nitropyrene; high performance liquid chromatography; peroxyoxalate-chemiluminescence detection; gasoline and diesel particulates;

D O I：

10.2116/analsci.7.Supple_1045

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A HPLC method with peroxyoxalate-chemiluminescence (CL) detection has been developed for the determination of dinitropyrenes (DNPs) and nitropyrene (NP). Both DNPs and NP, which are CL-insensitive, were initially reduced to the corresponding amino-derivatives with sodium hydrosulfide. They were separated on a reversed-phase column and chemilumigenically determined with detection limits in the subfmol range. Utilizing this method, DNPs and NP were determined in gasoline and diesel particulate samples.

引用

页码：1045 / 1048

页数：4

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