SEPARATION OF THE DIASTEREOISOMERS OF ETHYL-ESTERS OF CAFFEIC, FERULIC, AND ISOFERULIC ACIDS BY THIN-LAYER AND HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY

被引：16

作者：

BORGES, MFM

PINTO, MMM

机构：

[1] Laboratorio de Quimica Organica, Faculdade de Farmacia do Porto, Rua Anibal Cunha

来源：

JOURNAL OF LIQUID CHROMATOGRAPHY | 1994年 / 17卷 / 05期

关键词：

D O I：

10.1080/10826079408013390

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

The separation of the diastereoisomers of cinnamoyl derivatives have been studied by thin-layer (TLC) and high performance liquid chromatography (HPLC). TLC separations on two different layers and with two different solvent systems are described. HPLC separation was carried out on a reversed-phase column (Lichrosorb RP-8, 5 mu m) using an isocratic elution [acetonitrile : water-acetic acid (95 : 5)]. The series of compounds includes the cis/trans isomers of ethyl esters of caffeic, ferulic and isoferulic acids.

引用

页码：1125 / 1139

页数：15

共 8 条

[1] SYNTHESIS OF COUMARINS AND DERIVATIVES .1. BIOMIMETIC SYNTHESIS OF ESCULETIN AND HALOGENATED DERIVATIVES [J].