ANALYTICAL PERFORMANCE EVALUATION OF A 40.68 MHZ INDUCTIVELY COUPLED PLASMA MASS-SPECTROMETER

被引：12

作者：

PARK, CJ

LEE, KW

机构：

[1] Inorganic Analytical Laboratory, Korea Standards Research Institute, Taedok Science Town, Taejon

来源：

JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY | 1991年 / 6卷 / 06期

关键词：

INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY; 40.68 MHZ PLASMA; OPTIMIZATION AND ANALYTICAL PERFORMANCE; DETECTION LIMITS; BACKGROUND SPECTRUM;

D O I：

10.1039/ja9910600431

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The instrumentation of a new 40.68 MHz inductively coupled plasma (ICP) mass spectrometer is described. An optimization study has been carried out for the instrument. Of the many operating parameters, the carrier argon flow rate is the most sensitive and the optimum carrier argon flow rate is found to be much lower than the literature values for a 27.12 MHz ICP mass spectrometer. The analytical performance of the instrument, i.e., the detection limits, background mass spectrum and formation of oxides and doubly charged ions is also evaluated.

引用

页码：431 / 437

页数：7

共 19 条

[11] DETERMINATION OF THE RARE-EARTH ELEMENTS IN GEOLOGICAL-MATERIALS BY INDUCTIVELY COUPLED PLASMA MASS-SPECTROMETRY [J].

LICHTE, FE ;

MEIER, AL ;

CROCK, JG .

ANALYTICAL CHEMISTRY, 1987, 59 (08) :1150-1157

[12] LANGMUIR PROBE MEASUREMENTS OF POTENTIAL INSIDE A SUPERSONIC JET EXTRACTED FROM AN INDUCTIVELY COUPLED PLASMA [J].

LIM, HB ;

HOUK, RS ;

CRAIN, JS .

SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, 1989, 44 (10) :989-998

[13] OPTIMIZATION IN INDUCTIVELY COUPLED PLASMA MASS-SPECTROMETRY [J].

LONG, SE ;

BROWN, RM .

ANALYST, 1986, 111 (08) :901-906

[14]

PARK CJ, 1990, 5TH ANN M KOR SOC AN

[15] ANALYSIS OF LITHIUM AND BORON BY INDUCTIVELY COUPLED PLASMA MASS-SPECTROMETRY [J].

STOTESBURY, SJ ;

PICKERING, JM ;

GRIFFERTY, MA .

JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY, 1989, 4 (05) :457-460

[16] BACKGROUND SPECTRAL FEATURES IN INDUCTIVELY COUPLED PLASMA MASS-SPECTROMETRY [J].

TAN, SH ;

HORLICK, G .

APPLIED SPECTROSCOPY, 1986, 40 (04) :445-460

[17] OXIDE, HYDROXIDE, AND DOUBLY CHARGED ANALYTE SPECIES IN INDUCTIVELY COUPLED PLASMA MASS-SPECTROMETRY [J].

VAUGHAN, MA ;

HORLICK, G .

APPLIED SPECTROSCOPY, 1986, 40 (04) :434-445

[18] COMPARISON OF 27-MHZ AND 40-MHZ PLASMAS IN INDUCTIVELY COUPLED PLASMA MASS-SPECTROMETRY [J].

VICKERS, GH ;

WILSON, DA ;

HIEFTJE, GM .

JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY, 1989, 4 (08) :749-754

[19] ANALYTICAL CHARACTERISTICS OF AN INDUCTIVELY COUPLED PLASMA-MASS SPECTROMETER [J].

WILSON, DA ;

VICKERS, GH ;

HIEFTJE, GM ;

ZANDER, AT .

SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, 1987, 42 (1-2) :29-38

← 1 2 →