FORMATION OF SILICA-SURFACTANT MESOPHASES STUDIED BY REAL-TIME IN-SITU X-RAY-POWDER DIFFRACTION

被引：44

作者：

OBRIEN, S

FRANCIS, RJ

PRICE, SJ

OHARE, D

CLARK, SM

OKAZAKI, N

KURODA, K

机构：

[1] UNIV OXFORD,INORGAN CHEM LAB,OXFORD OX1 3QR,ENGLAND

[2] SERC,DARESBURY LAB,WARRINGTON WA4 4AD,CHESHIRE,ENGLAND

[3] WASEDA UNIV,DEPT APPL CHEM,SHINJUKU KU,TOKYO 169,JAPAN

[4] WASEDA UNIV,KAGAMI MEM LAB MAT SCI & TECHNOL,SHINJUKU KU,TOKYO 169,JAPAN

来源：

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS | 1995年 / 23期

关键词：

D O I：

10.1039/C39950002423

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Real-time in situ energy dispersive synchrotron X-ray powder diffraction data provides evidence for the formation of an intermediate lamellar silica-surfactant intercalate during the synthesis of the hexagonal-mesophase derived from the layered polysilicate kanemite, whereas no intermediate phases are observed during the formation of the silica-surfactant mesophase that leads to the mesoporous material MCM-41.

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页码：2423 / 2424

页数：2

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