SIMULTANEOUS STEREOANALYSIS OF 2-ALKYL-BRANCHED ACIDS, ESTERS AND ALCOHOLS USING A SELECTIVITY-ADJUSTED COLUMN SYSTEM IN MULTIDIMENSIONAL GAS-CHROMATOGRAPHY

被引：17

作者：

KARL, V ^{[1
]}

SCHMARR, HG ^{[1
]}

MOSANDL, A ^{[1
]}

机构：

[1] UNIV FRANKFURT,INST LEBENSMITTELCHEM,ROBERT MAYER STR 7-9,W-6000 FRANKFURT,GERMANY

来源：

JOURNAL OF CHROMATOGRAPHY | 1991年 / 587卷 / 02期

关键词：

D O I：

10.1016/0021-9673(91)85182-F

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The direct and simultaneous stereodifferentiation of 2-methylbutanoic acid, 2-methylbutanoic acid methyl and ethyl esters and the corresponding alcohol 2-methylbutane-1-ol from complex matrices is achieved, using selectivity-adjusted multi-dimensional gas chromatography with perethylated beta-cyclodextrin as the chiral stationary phase.

引用

页码：347 / 350

页数：4

共 12 条

[1] STEREODIFFERENTIATION OF SOME CHIRAL MONOTERPENES USING MULTIDIMENSIONAL GAS-CHROMATOGRAPHY
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[7] MOSANDL A, 1990, DEUT LEBENSM-RUNDSCH, V86, P375
[8] NOWOTNY HP, 1989, HRC-J HIGH RES CHROM, V12, P383
[9] CHIROSPECIFIC ANALYSIS OF 2-ALKYL-BRANCHED ALCOHOLS, ACIDS, AND ESTERS - CHIRALITY EVALUATION OF 2-METHYLBUTANOATES FROM APPLES AND PINEAPPLES
RETTINGER, K
KARL, V
SCHMARR, HG
DETTMAR, F
HENER, U
MOSANDL, A
[J]. PHYTOCHEMICAL ANALYSIS, 1991, 2 (04) : 184 - 188
[10] MULTIDIMENSIONAL CAPILLARY GAS-CHROMATOGRAPHY - ENANTIOMERIC SEPARATIONS OF SELECTED CUTS USING A CHIRAL 2ND COLUMN
SCHOMBURG, G
HUSMANM, H
HUBINGER, E
KONIG, WA
[J]. JOURNAL OF HIGH RESOLUTION CHROMATOGRAPHY & CHROMATOGRAPHY COMMUNICATIONS, 1984, 7 (07): : 404 - 410

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