CHARACTERIZATION OF THE CHEMICAL BONDING IN INNER LAYERS OF COMPOSITE-MATERIALS

被引:8
作者
SCHNEIDER, R [1 ]
WOLTERSDORF, J [1 ]
RODER, A [1 ]
机构
[1] UNIV HALLE WITTENBERG,FACHBEREICH PHYS,D-06108 HALLE,GERMANY
来源
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1995年 / 353卷 / 3-4期
关键词
D O I
10.1007/BF00322049
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The efficiency of near edge structure investigations in electron energy loss spectroscopy (EELS) is discussed for characterizing the chemical bonding of elements present in the interfacial zone in fibre/matrix composites at nanometre resolution. Two different examples of corresponding analyses are given for a SiC-fibre reinforced borosilicate glass. In particular, the chemical bonding between silicon and carbon or oxygen (e.g. SiC, SiO2 and SiOxCy), respectively, is characterized. The results have been attained in a fingerprint manner by comparing the fine structure measured from a material of unknown stoichiometry to that of a standard specimen. In addition, a possibility is demonstrated to image the chemical bonding by energy-filtered microscopy using energy loss near edge structures (ELNES).
引用
收藏
页码:263 / 266
页数:4
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