CHIRAL HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY WITH CELLULOSE CARBAMATE-COATED PHASES - INFLUENCE OF SUPPORT SURFACE-CHEMISTRY ON ENANTIOSELECTIVITY

被引：37

作者：

GRIEB, SJ

MATLIN, SA

BELENGUER, AM

RITCHIE, HJ

机构：

[1] UNIV WARWICK,DEPT CHEM,COVENTRY CV4 7AL,W MIDLANDS,ENGLAND

[2] SB PHARMACEUT,TONBRIDGE TN11 9AN,KENT,ENGLAND

[3] SHANDON HPLC,RUNCORN WA7 1PR,CHESHIRE,ENGLAND

来源：

JOURNAL OF CHROMATOGRAPHY A | 1995年 / 697卷 / 1-2期

基金：

英国工程与自然科学研究理事会;

关键词：

D O I：

10.1016/0021-9673(94)00868-A

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

The influence of support surface chemistry on the enantioselectivity and column performance of cellulose tris(3,5-dimethylphenyl carbamate)-coated chiral HPLC phases was investigated. Stable coated phases were produced using underivatised, aminopropylated and octadecylated silica as the support media. For many racemates, underivatised silica at a 20% (w/w) loading was found to be the most efficient phase.

引用

页码：271 / 278

页数：8

共 12 条

[1] ROLE OF SOLVENTS IN THE RESOLUTION OF SOME BETA-ADRENERGIC BLOCKERS ON CELLULOSE 3,5-DIMETHYLPHENYL CARBAMATE CHIRAL STATIONARY PHASE
ABOULENEIN, HY
SERIGNESE, V
[J]. JOURNAL OF LIQUID CHROMATOGRAPHY, 1993, 16 (01): : 197 - 207
[2] CHIRAL PACKING MATERIALS FOR HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC RESOLUTION OF ENANTIOMERS BASED ON SUBSTITUTED BRANCHED POLYSACCHARIDES COATED ON SILICA-GEL
FELIX, G
ZHANG, T
[J]. JOURNAL OF CHROMATOGRAPHY, 1993, 639 (02): : 141 - 149
[3] CHIRAL HPLC WITH CARBOHYDRATE CARBAMATES - INFLUENCE OF SUPPORT STRUCTURE ON ENANTIOSELECTIVITY
GRIEB, SJ
MATLIN, SA
PHILLIPS, JG
BELENGUER, AM
RITCHIE, HJ
[J]. CHIRALITY, 1994, 6 (02) : 129 - 134
[4] HPLC WITH CARBOHYDRATE CARBAMATE CHIRAL PHASES - INFLUENCE OF CHIRAL PHASE-STRUCTURE ON ENANTIOSELECTIVITY
MATLIN, SA
TIRITAN, ME
CRAWFORD, AJ
CASS, QB
BOYD, DR
[J]. CHIRALITY, 1994, 6 (02) : 135 - 140
[5] CHROMATOGRAPHIC RESOLUTION .12. OPTICAL RESOLUTION OF BETA-BLOCKERS BY HPLC ON CELLULOSE TRIPHENYLCARBAMATE DERIVATIVES
OKAMOTO, Y
KAWASHIMA, M
ABURATANI, R
HATADA, K
NISHIYAMA, T
MASUDA, M
[J]. CHEMISTRY LETTERS, 1986, (07) : 1237 - 1240
[6] CHROMATOGRAPHIC RESOLUTION .17. USEFUL CHIRAL STATIONARY PHASES FOR HPLC - AMYLOSE TRIS(3,5-DIMETHYLPHENYLCARBAMATE) AND TRIS(3,5-DICHLOROPHENYLCARBAMATE) SUPPORTED ON SILICA-GEL
OKAMOTO, Y
ABURATANI, R
FUKUMOTO, T
HATADA, K
[J]. CHEMISTRY LETTERS, 1987, (09) : 1857 - 1860
[7] CHROMATOGRAPHIC RESOLUTION .19. DIRECT OPTICAL RESOLUTION OF CARBOXYLIC-ACIDS BY CHIRAL HPLC ON TRIS(3,5-DIMETHYLPHENYLCARBAMATE)S OF CELLULOSE AND AMYLOSE
OKAMOTO, Y
ABURATANI, R
KAIDA, Y
HATADA, K
[J]. CHEMISTRY LETTERS, 1988, (07) : 1125 - 1128
[8] DIRECT CHROMATOGRAPHIC-SEPARATION OF 2-ARYLPROPIONIC ACID ENANTIOMERS USING TRIS(3,5-DIMETHYLPHENYLCARBAMATE)S OF CELLULOSE AND AMYLOSE AS CHIRAL STATIONARY PHASES
OKAMOTO, Y
ABURATANI, R
KAIDA, Y
HATADA, K
INOTSUME, N
NAKANO, M
[J]. CHIRALITY, 1989, 1 (03) : 239 - 242
[9] OPTICAL RESOLUTION OF RACEMIC DRUGS BY CHIRAL HPLC ON CELLULOSE AND AMYLOSE TRIS(PHENYLCARBAMATE) DERIVATIVES
OKAMOTO, Y
ABURATANI, R
HATANO, K
HATADA, K
[J]. JOURNAL OF LIQUID CHROMATOGRAPHY, 1988, 11 (9-10): : 2147 - 2163
[10] CHROMATOGRAPHIC RESOLUTION .11. CONTROLLED CHIRAL RECOGNITION OF CELLULOSE TRIPHENYLCARBAMATE DERIVATIVES SUPPORTED ON SILICA-GEL
OKAMOTO, Y
KAWASHIMA, M
HATADA, K
[J]. JOURNAL OF CHROMATOGRAPHY, 1986, 363 (02): : 173 - 186

← 1 2 →