CHARACTERIZATION OF NANOPHASE POWDERS PREPARED BY LASER SYNTHESIS

被引:5
作者
GIORGI, R [1 ]
MARTELLI, S [1 ]
TURTU, S [1 ]
ZAPPA, G [1 ]
BORSELLA, E [1 ]
BOTTI, S [1 ]
机构
[1] ENEA,DIPARTIMENTO INNOVAZ,SETTORE ELETTROOTT & LASER,I-00044 FRASCATI,ITALY
关键词
D O I
10.1002/sia.740220154
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Si-based (Si-C-N and Si-C-Al) nanopowders prepared by laser synthesis process have been studied by XPS and XAES analyses. The changes of the silicon coordination as a function of the carbon fraction in Si-C-N powders have been investigated by a detailed analysis of Si 2p and Si KLL lines and the measurements of the Auger parameter E(k)(Si KLL) + E(b)(Si 2p). The non-linear dependence of the Auger parameter on the carbon fraction has been interpreted as due to the formation of a carbonitride nanophase, indicating that the ternary powders are not merely a mixture of silicon carbide and silicon nitride. In Si-C-Al powders it has been found that the incorporation of aluminium results in a modified structure of the silicon carbide, as shown by the variation of the different spectral features.
引用
收藏
页码:248 / 253
页数:6
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