SYNTHESIS AND CHARACTERIZATION OF STATIONARY PHASES ON THE BASIS OF SILICAS MODIFIED WITH EPOXIDIZED POLYBUTADIENES - SYNTHESIS AND CHARACTERIZATION OF A NEW POLYHYDROXY FUNCTIONALIZED STATIONARY PHASE FOR HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY .1.

被引：6

作者：

ERLER, U

SPANGE, S

HEUBLEIN, G

机构：

[1] Friedrich-Schiller-Universität, Sektion Chemie, Jena

来源：

ACTA POLYMERICA | 1991年 / 42卷 / 08期

关键词：

D O I：

10.1002/actp.1991.010420811

中图分类号：

O63 [高分子化学（高聚物）];

学科分类号：

070305 ; 080501 ; 081704 ;

摘要：

A new polyhydroxy functionalized support, derived front reaction composites of epoxidized polybutadienes and silicas, is tested as a stationary phase for high performance liquid chromatography. As demonstrated in various chromatographic separations, the retention behaviour of different test solutes depends on their polarity and hydrogen bond forming ability. A number of phenolic compounds, xanthine derivatives, and steroid samples is chromatographed under isocratic conditions with hexane, methanol and THF as eluents.

引用

收藏

页码：389 / 393

页数：5

相关论文

共 36 条

[11] REACTION COMPOSITES FROM POLYFUNCTIONAL MACROMOLECULES AND INORGANIC SOLIDS [J].

HEUBLEIN, G ;

HEUBLEIN, B ;

HORTSCHANSKY, P ;

MEISSNER, H ;

SCHUTZ, H .

JOURNAL OF MACROMOLECULAR SCIENCE-CHEMISTRY, 1988, A25 (02) :183-200

[12] SYNTHESIS AND CHARACTERIZATION OF STATIONARY PHASES BASED ON POLYSILICIC ACIDS MODIFIED WITH EPOXIDIZED POLYBUTADIENE (PBDE) .1. STUDIES ON THE SURFACE MODIFICATION OF POLYSILICIC ACIDS WITH EPOXIDIZED POLYBUTADIENES [J].

HEUBLEIN, G ;

ERLER, U ;

ULBRICHT, A ;

WINKELMANN, H .

ANGEWANDTE MAKROMOLEKULARE CHEMIE, 1990, 182 :29-42

[13]

HEUBLEIN G, 1989, MAKROMOL CHEM, V190, P9

[14] HYDROGEN BONDING INTERACTIONS OF PARA NITROPHENOL [J].

HUDSON, RA ;

SCOTT, RM ;

VINOGRADOV, SN .

SPECTROCHIMICA ACTA PART A-MOLECULAR SPECTROSCOPY, 1970, A 26 (02) :337-+

[15] CHROMATOGRAPHY IN STEROID RESEARCH WORK [J].

IKEKAWA, N .

TRAC-TRENDS IN ANALYTICAL CHEMISTRY, 1984, 3 (03) :81-87

[16] POLYMER-COATED CATION-EXCHANGE STATIONARY PHASES ON THE BASIS OF SILICA [J].

KOLLA, P ;

KOHLER, J ;

SCHOMBURG, G .

CHROMATOGRAPHIA, 1987, 23 (07) :465-472

[17] HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY OF NATURALLY-OCCURRING ESTROGENS [J].

LIN, JT ;

HEFTMANN, E .

JOURNAL OF CHROMATOGRAPHY, 1981, 212 (02) :239-244

[18] LINEAR RELATIONSHIP BETWEEN THE LOGARITHM OF THE EQUILIBRIUM-CONSTANTS AND THE LOGARITHM OF THE LIQUID-CHROMATOGRAPHIC SEPARATION FACTORS FOR TAUTOMERS OBTAINED IN DIFFERENT SOLVENTS [J].

OKA, K ;

HARA, S .

JOURNAL OF CHROMATOGRAPHY, 1980, 202 (02) :187-194

[19] ACID STRENGTHS OF SOME SUBSTITUTED PICRIC ACIDS [J].

PEARCE, PJ ;

SIMKINS, RJJ .

CANADIAN JOURNAL OF CHEMISTRY, 1968, 46 (02) :241-&

[20] USE OF GRADIENT ELUTION FOR RAPID SELECTION OF ISOCRATIC CONDITIONS IN REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY [J].

SCHOENMAKERS, PJ ;

BILLIET, HAH ;

DEGALAN, L .

JOURNAL OF CHROMATOGRAPHY, 1981, 205 (01) :13-30

← 1 2 3 4 →