REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC METHOD USING A PENTAFLUOROPHENYL BONDED PHASE FOR ANALYSIS OF TOCOPHEROLS

被引:61
作者
RICHHEIMER, SL
KENT, MC
BERNART, MW
机构
[1] Hauser Chemical Research, Inc., Boulder, CO 80301
关键词
D O I
10.1016/0021-9673(94)80546-6
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
A high-performance liquid chromatographic (HPLC) method to determine four tocopherols (alpha-, beta-, gamma-, and delta-) simultaneously was developed using a pentafluorophenyl reversed-phase column. A mobile phase of 92% aqueous methanol was used. Tocopherols were measured in vegetable oil, soybean oil deodorizer distillate, mixed tocopherol concentrate, and vitamin E pharmaceutical preparations.
引用
收藏
页码:75 / 80
页数:6
相关论文
共 19 条
[1]   SIMULTANEOUS ANALYSIS OF INDIVIDUAL CAROTENOIDS, RETINOL, RETINYL ESTERS, AND TOCOPHEROLS IN SERUM BY ISOCRATIC NONAQUEOUS REVERSED-PHASE HPLC [J].
BARUA, AB ;
FURR, HC ;
JANICKBUCKNER, D ;
OLSON, JA .
FOOD CHEMISTRY, 1993, 46 (04) :419-424
[2]   PREPARATION AND COMPARISON OF A PENTAFLUOROPHENYL STATIONARY PHASE FOR REVERSED-PHASE LIQUID-CHROMATOGRAPHY [J].
CSATO, E ;
FULOP, N ;
SZABO, G .
JOURNAL OF CHROMATOGRAPHY, 1990, 511 :79-88
[3]  
HAAS A, 1981, CHROMATOGRAPHIA, V6, P341
[4]  
HORWITZ W, 1975, OFFICIAL METHODS ANA, P836
[5]   SEPARATION AND IDENTIFICATION OF CAROTENOIDS AND THEIR OXIDATION-PRODUCTS IN THE EXTRACTS OF HUMAN PLASMA [J].
KHACHIK, F ;
BEECHER, GR ;
GOLI, MB ;
LUSBY, WR ;
SMITH, JC .
ANALYTICAL CHEMISTRY, 1992, 64 (18) :2111-2122
[6]   CAROTENOID AND TOCOPHEROL COMPOSITION OF HUMAN ADIPOSE-TISSUE [J].
PARKER, RS .
AMERICAN JOURNAL OF CLINICAL NUTRITION, 1988, 47 (01) :33-36
[7]   DETERMINATION OF TOCOPHEROLS AND TOCOTRIENOLS IN VEGETABLE-OILS AND FATS BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY - RESULTS OF A COLLABORATIVE STUDY AND THE STANDARDIZED METHOD [J].
POCKLINGTON, WD ;
DIEFFENBACHER, A .
PURE AND APPLIED CHEMISTRY, 1988, 60 (06) :877-892
[8]   SEPARATION OF TOCOLS BY HPLC ON AN AMINO-CYANO POLAR PHASE COLUMN [J].
RAMMELL, CG ;
HOOGENBOOM, JJL .
JOURNAL OF LIQUID CHROMATOGRAPHY, 1985, 8 (04) :707-717
[9]   HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC ASSAY OF TAXOL [J].
RICHHEIMER, SL ;
TINNERMEIER, DM ;
TIMMONS, DW .
ANALYTICAL CHEMISTRY, 1992, 64 (20) :2323-2326
[10]   IDENTIFICATION AND QUANTITATION OF GAMMA-ORYZANOL COMPONENTS AND SIMULTANEOUS ASSESSMENT OF TOCOLS IN RICE BRAN OIL [J].
ROGERS, EJ ;
RICE, SM ;
NICOLOSI, RJ ;
CARPENTER, DR ;
MCCLELLAND, CA ;
ROMANCZYK, LJ .
JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY, 1993, 70 (03) :301-307