PREPARATIVE SEPARATION OF FULLERENE ADDUCTS BY LIQUID-CHROMATOGRAPHY ON POLYSTYRENE GEL

被引：11

作者：

GUGEL, A

MULLEN, K

机构：

[1] Max-Planck-Institut für Polymerforschung, Mainz

来源：

CHROMATOGRAPHIA | 1993年 / 37卷 / 7-8期

关键词：

COLUMN LIQUID CHROMATOGRAPHY; FULLERENES; FULLERENE ADDUCTS; POLYSTYRENE GEL; PREPARATIVE SCALE SEPARATIONS;

D O I：

10.1007/BF02272253

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

The preparative separation of numerous fullerene adducts by liquid chromatography on polystyrene gel is described. These adducts can be resolved on a scale of 10-40 g/day on a 600 x 20 mm column. Both toluene and chloroform can be used as mobile phases; toluene offers better solubility for the adducts and chloroform better peak resolution.

引用

页码：387 / 391

页数：5

共 22 条

[1]

ALTGELT KH, 1971, GEL PERMEATION CHROM

[2] RING INVERSION IN CYCLOHEXENE [J].

ANET, FAL ;

HAQ, MZ .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1965, 87 (14) :3147-&

[3]

DETERMANN H, 1967, GELCHROMATOGRAPHIE

[4]

ELEMES Y, 1992, ANGEW CHEM, V104, P364

[5] SEPARATION OF C-60 AND C-70 ON POLYSTYRENE GEL WITH TOLUENE AS MOBILE PHASE [J].

GUGEL, A ;

MULLEN, K .

JOURNAL OF CHROMATOGRAPHY, 1993, 628 (01) :23-29

[6]

GUGEL A, UNPUB

[7]

GUGEL A, 1992, ANGEW CHEM, V104, P666

[8] TITRATION OF C-60 - A METHOD FOR THE SYNTHESIS OF ORGANOFULLERENES [J].

HIRSCH, A ;

SOI, A ;

KARFUNKEL, HR .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1992, 31 (06) :766-768

[9]

HIRSCH A, 1992, ANGEW CHEM, V104, P808

[10]

Hunt B. J., 1989, SIZE EXCLUSION CHROM

← 1 2 3 →