Synthesis and crystal structure of the first d-f heterodinuclear Dy(III)-Cu(II) cryptate

被引:44
作者
Chen, QY [1 ]
Luo, QH
Wang, ZL
Chen, JT
机构
[1] Nanjing Univ, Inst Coordinat Chem, Nanjing 210093, Peoples R China
[2] Nanjing Univ, State Key Lab Coordinat Chem, Nanjing 210093, Peoples R China
[3] Fuzhou State Key Lab Struct Chem, Fuzhou 350002, Peoples R China
关键词
D O I
10.1039/a909926n
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The heterodinuclear cryptate [DyCuL(DMF)](ClO4)(2). MeCN [where L denotes the deprotonated anionic cryptand obtained by condensation of tris(2-aminoethyl)amine with 2,6-diformyl-4-chlorophenol] has been obtained by a stepwise method; the presence of copper(ii) and dysprosium(iii) in the cavity of the cryptand was evidenced by X-ray structure analysis and ESMS spectroscopy.
引用
收藏
页码:1033 / 1034
页数:2
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