Material anisotropy revealed by phase contrast in intermittent contact atomic force microscopy

被引:39
作者
Marcus, MS
Carpick, RW
Sasaki, DY
Eriksson, MA
机构
[1] Univ Wisconsin, Dept Phys, Madison, WI 53706 USA
[2] Univ Wisconsin, Dept Engn Phys, Mat Sci Program, Madison, WI 53706 USA
[3] Univ Wisconsin, Rheol Res Ctr, Madison, WI 53706 USA
[4] Sandia Natl Labs, Biomol Mat & Interface Sci Dept, Albuquerque, NM 87185 USA
关键词
D O I
10.1103/PhysRevLett.88.226103
中图分类号
O4 [物理学];
学科分类号
0702 ;
摘要
Phase contrast in intermittent-contact atomic force microscopy (AFM) reveals in-plane structural and mechanical properties of polymer monolayers. This is surprising, because measurements of nanoscale in-plane properties typically require contact mode microscopies. Our measurements are possible because the tip oscillates not just perpendicular but also parallel to the sample surface along the long axis of the cantilever. This lateral tip displacement is virtually universal in AFM, implying that any oscillating-tip AFM technique is sensitive to in-plane material properties.
引用
收藏
页码:4 / 226103
页数:4
相关论文
共 32 条
[1]   Influence of noncontact dissipation in the tapping mode:: Attempt to extract quantitative information on the surface properties with the local force probe method [J].
Aimé, JP ;
Boisgard, R ;
Nony, L ;
Couturier, G .
JOURNAL OF CHEMICAL PHYSICS, 2001, 114 (11) :4945-4954
[2]   Anisotropic nanoindentation of transcrystalline polypropylene by scanning force microscope using blade-like tips [J].
Amitay-Sadovsky, E ;
Cohen, SR ;
Wagner, HD .
APPLIED PHYSICS LETTERS, 1999, 74 (20) :2966-2968
[3]   Phase imaging: Deep or superficial? [J].
Behrend, OP ;
Odoni, L ;
Loubet, JL ;
Burnham, NA .
APPLIED PHYSICS LETTERS, 1999, 75 (17) :2551-2553
[4]   Intermittent contact: tapping or hammering? [J].
Behrend, OP ;
Oulevey, F ;
Gourdon, D ;
Dupas, E ;
Kulik, AJ ;
Gremaud, G ;
Burnham, NA .
APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING, 1998, 66 (Suppl 1) :S219-S221
[5]   A simplified but intuitive analytical model for intermittent-contact-mode force microscopy based on Hertzian mechanics [J].
Bielefeldt, H ;
Giessibl, FJ .
SURFACE SCIENCE, 1999, 440 (03) :L863-L867
[6]  
BLUHM H, 1995, APPL PHYS A-MATER, V61, P525, DOI 10.1007/BF01540254
[7]   How does a tip tap? [J].
Burnham, NA ;
Behrend, OP ;
Oulevey, F ;
Gremaud, G ;
Gallo, PJ ;
Gourdon, D ;
Dupas, E ;
Kulik, AJ ;
Pollock, HM ;
Briggs, GAD .
NANOTECHNOLOGY, 1997, 8 (02) :67-75
[8]   Molecular level friction as revealed with a novel scanning probe [J].
Burns, AR ;
Houston, JE ;
Carpick, RW ;
Michalske, TA .
LANGMUIR, 1999, 15 (08) :2922-2930
[9]   Directional shear force microscopy [J].
Burns, AR ;
Carpick, RW .
APPLIED PHYSICS LETTERS, 2001, 78 (03) :317-319
[10]   Lateral stiffness: A new nanomechanical measurement for the determination of shear strengths with friction force microscopy [J].
Carpick, RW ;
Ogletree, DF ;
Salmeron, M .
APPLIED PHYSICS LETTERS, 1997, 70 (12) :1548-1550