A versatile sample-environment cell for non-ambient X-ray scattering experiments

被引:264
作者
Chupas, Peter J. [1 ]
Chapman, Karena W. [1 ]
Kurtz, Charles [1 ]
Hanson, Jonathan C. [2 ]
Lee, Peter L. [1 ]
Grey, Clare P. [3 ]
机构
[1] Argonne Natl Lab, Xray Sci Div, Argonne, IL 60439 USA
[2] Brookhaven Natl Lab, Dept Chem, Upton, NY 11973 USA
[3] SUNY Stony Brook, Dept Chem, Stony Brook, NY 11794 USA
关键词
D O I
10.1107/S0021889808020165
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A compact reaction cell is described for in-situ experiments requiring control of both the temperature of the sample and the atmosphere over the sample. The cell incorporates an optional furnace capable of temperatures of up to similar to 1273 K. The compact design and ability of the cell to mount directly on a standard goniometer head allows portability to a large number of diffraction instruments at synchrotron sources.
引用
收藏
页码:822 / 824
页数:3
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