On the use of grazing-incidence small-angle X-ray scattering (GISAXS) in the morphological study of ion-implanted materials

被引:6
作者
d'Acapito, F
Maurizio, C
Gonella, F
Cattaruzza, E
Mattei, G
Mondelli, C
Longo, A
Martorana, A
机构
[1] European Synchrotron Radiat Facil, INFM, OGG, GILDA CRG, F-38043 Grenoble, France
[2] Univ Venice, Dipartimento Chim Fis, I-30123 Venice, Italy
[3] Univ Padua, Dipartimento Fis, I-35131 Padua, Italy
[4] INFM, OGG, ILL, F-38042 Grenoble, France
[5] CNR, ICTPN, I-90146 Palermo, Italy
[6] Univ Palermo, Dipartimento Chim Inorgan, I-90128 Palermo, Italy
关键词
grazing-incidence small-angle X-ray scattering; ion implantation; metallic nanoparticles; glass-nanocluster composites; small-angle neutron scattering;
D O I
10.1107/S0909049504002523
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
Grazing-incidence small-angle X-ray scattering has become a widely used technique for the morphological analysis of surface systems. Here it is show how this technique can be applied to a buried system, like metallic clusters in glass obtained by ion implantation. The optimization of the data-collection geometry is described as well as the details of the quantitative data analysis. An experimental example on Cu+Au-implanted glasses shows the potentiality of the technique.
引用
收藏
页码:272 / 277
页数:6
相关论文
共 41 条
[1]   Semiconductor clusters, nanocrystals, and quantum dots [J].
Alivisatos, AP .
SCIENCE, 1996, 271 (5251) :933-937
[2]   STRUCTURE AND RESISTIVITY OF LIQUID METALS [J].
ASHCROFT, NW ;
LEKNER, J .
PHYSICAL REVIEW, 1966, 145 (01) :83-&
[3]   Morphological characterization of ion-sputtered C-Ag C/C-Ag and Ag/C films by GISAXS [J].
Babonneau, D ;
Naudon, A ;
Thiaudière, D ;
Lequien, S .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1999, 32 :226-233
[4]   Morphology and size distribution of gold nanoclusters in a-C:H films studied by grazing incidence small-angle x-ray scattering -: art. no. 195401 [J].
Babonneau, D ;
Videnovic, IR ;
Garnier, MG ;
Oelhafen, P .
PHYSICAL REVIEW B, 2001, 63 (19)
[5]   A MONTE-CARLO COMPUTER-PROGRAM FOR THE TRANSPORT OF ENERGETIC IONS IN AMORPHOUS TARGETS [J].
BIERSACK, JP ;
HAGGMARK, LG .
NUCLEAR INSTRUMENTS & METHODS, 1980, 174 (1-2) :257-269
[6]   Quantum-dot composite silicate glasses obtained by ion implantation [J].
Cattaruzza, E .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 2000, 169 :141-155
[7]   GISAXS study of Cu-Ni alloy clusters obtained by double ion implantation in silicate glasses [J].
Cattaruzza, E ;
d'Acapito, F ;
Gonella, F ;
Longo, A ;
Martorana, A ;
Mattei, G ;
Maurizio, C ;
Thiaudière, D .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2000, 33 (01) :740-743
[8]  
*CERN, 1994, MINUIT CERN PROGR LI
[9]   Structural characterization of Cu metallic clusters in amorphous SiO2 by synchrotron radiation grazing incidence X-ray scattering and diffraction [J].
D'Acapito, F ;
Thiaudiere, D ;
Zontone, F ;
Regnard, JR .
EPDIC 5, PTS 1 AND 2, 1998, 278-2 :891-896
[10]   Valence state and local atomic structure of copper in Cu-implanted silica glass [J].
d'Acapito, F ;
Mobilio, S ;
Battaglin, G ;
Cattaruzza, E ;
Gonella, F ;
Caccavale, F ;
Mazzoldi, P ;
Regnard, JR .
JOURNAL OF APPLIED PHYSICS, 2000, 87 (04) :1819-1824