Low temperature fabrication and impedance spectroscopy of PMN-PT ceramics

被引:127
作者
James, AR
Srinivas, K
机构
[1] Indian Inst Sci, Mat Res Ctr, Bangalore 560012, Karnataka, India
[2] Osmania Univ, Dept Phys, Hyderabad 500007, Andhra Pradesh, India
关键词
ceramics; electron microscopy; impedance spectroscopy; X-ray diffraction; electrical properties;
D O I
10.1016/S0025-5408(99)00127-0
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Single phase perovskite 0.9Pb(Mg1/3Nb2/3)O-3-0.1(PbTiO3) ceramics were prepared using the columbite precursor method after optimizing the synthesis conditions. X-ray diffraction (XRD) studies were carried out to verify the phase formation at each processing step. Scanning electron microscopy (SEM) was employed to observe the microstructure of the sintered ceramics. Impedance and modulus spectroscopic data were used to gain an insight into the electrical properties of the samples and with a view to observing the relaxations in them. (C) 1999 Elsevier Science Ltd.
引用
收藏
页码:1301 / 1310
页数:10
相关论文
共 14 条
[1]   IMPEDANCE AND DIELECTRIC-SPECTROSCOPY REVISITED - DISTINGUISHING LOCALIZED RELAXATION FROM LONG-RANGE CONDUCTIVITY [J].
GERHARDT, R .
JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 1994, 55 (12) :1491-1506
[2]   Impedance spectroscopy of undoped BaTiO3 ceramics [J].
Hirose, N ;
West, AR .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1996, 79 (06) :1633-1641
[3]   IMPEDANCE SPECTROSCOPIC STUDIES IN SrBi5FeTi4O18 [J].
James, A. R. ;
Kumar, G. S. ;
Suryanarayana, S. V. ;
Bhimasankaram, T. .
FERROELECTRICS, 1996, 189 :81-90
[4]   The dielectric and electrical properties of four layered LaBi4FeTi3O15 [J].
James, AR ;
Kumar, GS ;
Suryanarayana, SV ;
Bhimasankaram, T .
FERROELECTRICS, 1998, 216 (1-4) :11-26
[5]  
Jonscher A. K., 1980, PHYS THIN FILMS, V11, P205
[6]  
LEJUENE M, 1983, CERAM INT, V9, P119
[7]  
MACDONALD JR, 1976, SUPERIONIC CONDUCTOR
[8]  
MIYASAKA Y, 1990, P 7 INT S APPL FERR, P121
[9]   EFFECT OF ATMOSPHERE ON THE PTCR PROPERTIES OF BATIO3 CERAMICS [J].
SINCLAIR, DC ;
WEST, AR .
JOURNAL OF MATERIALS SCIENCE, 1994, 29 (23) :6061-6068
[10]   FABRICATION OF PEROVSKITE LEAD MAGNESIUM NIOBATE [J].
SWARTZ, SL ;
SHROUT, TR .
MATERIALS RESEARCH BULLETIN, 1982, 17 (10) :1245-1250