Solventless synthesis of thiohydantoins over K2CO3

被引：112

作者：

Kidwai, M ^{[1
]}

Venkataramanan, R ^{[1
]}

Dave, B ^{[1
]}

机构：

[1] Univ Delhi, Dept Chem, Delhi 110007, India

来源：

GREEN CHEMISTRY | 2001年 / 3卷 / 06期

关键词：

D O I：

10.1039/b106034c

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Potassium carbonate supported solventless synthesis of thiohydantoins under microwave irradiation is described. The use of K2CO3 not only eliminates the need for external base to neutralize HCl evolved but enables aqueous work up, thus rendering the reaction procedure free of organic solvents in both the reaction step and work-up, procedure.

引用

页码：278 / 279

页数：2

共 16 条

[1]

ARNOLD H, 1962, Patent No. 1135915

[2] STUDY OF 5-ARYLIDENE-2-THIOHYDANTOINS WITH POTENTIAL IMMUNOMODULATING AND ANTICANCER ACTIVITIES [J].