Heterocycloaddition of thermally generated 1,2-diaza-1,3-butadienes to [60]fullerene

被引：24

作者：

Yang, Hai-Tao

Wang, Guan-Wu ^{[1
]}

Xu, Yu

Huang, Jin-Chang

机构：

[1] Univ Sci & Technol China, Hafei Natl Lab Phys Sci Microscale, Hefei 230026, Anhui, Peoples R China

[2] Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China

来源：

TETRAHEDRON LETTERS | 2006年 / 47卷 / 25期

基金：

中国国家自然科学基金;

关键词：

60]Fullerene; Hetero-Diels-Alder reaction; 1,2-diaza-1,3-butachenes;

D O I：

10.1016/j.tetlet.2006.04.034

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Stable C-60-fused tetrahydropitridazine derivatives were synthesized through the hetero-Diels-Alder cycloaddition of C-60 with 1,2-diaza-1,3-butadienes, which were generated in situ by the thermal extrusion of sulfur dioxide from 2,5-dihydro-1,2,3-thiadiazole- 1,1-dioxides. (c) 2006 Elsevier Ltd. All rights reserved.

引用

页码：4129 / 4131

页数：3

共 27 条

[1] REARRANGEMENT REACTIONS .3. SYNTHESES AND DIELS-ALDER REACTIONS OF 2-ALKYLAZO-SUBSTITUTED 1,3-BUTADIENES
BANERT, K
HAGEDORN, M
[J]. TETRAHEDRON LETTERS, 1992, 33 (48) : 7331 - 7334
[2] REACTION OF BUCKMINSTERFULLERENE WITH ORTHO-QUINODIMETHANE - A NEW ACCESS TO STABLE C60 DERIVATIVES
BELIK, P
GUGEL, A
SPICKERMANN, J
MULLEN, K
[J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1993, 32 (01): : 78 - 80
[3] New heterocyclic precursors for thermal generation of reactive, electron-rich 1,2-diaza-1 3-butadienes
Boeckman, RK
Ge, P
Reed, JE
[J]. ORGANIC LETTERS, 2001, 3 (23) : 3647 - 3650
[4] Fullerene derivatives: an attractive tool for biological applications
Bosi, S
Da Ros, T
Spalluto, G
Prato, M
[J]. EUROPEAN JOURNAL OF MEDICINAL CHEMISTRY, 2003, 38 (11-12) : 913 - 923
[5] CAGLIOTI L, 1970, TETRAHEDRON LETT, V27, P2349
[6] One-pot sequential synthesis of acetoxylated [60]fullerene derivatives
Chen, ZX
Wang, GW
[J]. JOURNAL OF ORGANIC CHEMISTRY, 2005, 70 (06) : 2380 - 2383
[7] CYCLO-ADDITION REACTIONS OF NITROSOALKENES AND AZOALKENES WITH CYCLOPENTADIENE AND OTHER DIENES
FARAGHER, R
GILCHRIST, TL
[J]. JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1979, (01): : 249 - 257
[8] SELECTIVE REDUCTION AND CLEAVAGE OF THE N-N BOND OF FUSED TETRAHYDROPYRIDAZINES - A ROUTE TO FUNCTIONALIZED LACTAMS
GILCHRIST, TL
HUGHES, D
WASSON, R
[J]. TETRAHEDRON LETTERS, 1987, 28 (14) : 1573 - 1576
[9] GILCHRIST TL, 1983, SYNTHESIS-STUTTGART, P153
[10] INTRAMOLECULAR CYCLO-ADDITION OF AZOALKENES DERIVED FROM ALLYLIC BETA-KETO-ESTERS
GILCHRIST, TL
ROMERO, OAS
WASSON, RC
[J]. JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1989, (02): : 353 - 359

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