Zinc Glycolate: A Precursor to ZnO

被引：60

作者：

Das, Jaykrushna ^{[1
]}

Evans, Ivana R. ^{[2
]}

Khushalani, Deepa ^{[1
]}

机构：

[1] Tata Inst Fundamental Res, Dept Chem Sci, Mat Chem Grp, Bombay 400005, Maharashtra, India

[2] Univ Durham, Dept Chem, Durham DH1 3LE, England

来源：

INORGANIC CHEMISTRY | 2009年 / 48卷 / 08期

基金：

英国工程与自然科学研究理事会;

关键词：

PHOTOCATALYTIC ACTIVITY; NANOPARTICLES; PHOTOLUMINESCENCE; LUMINESCENCE; GROWTH; ARRAYS;

D O I：

10.1021/ic900067w

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A simple and versatile solvent-growth process using ethylene glycol has been demonstrated for the synthesis of novel faceted bipyramidal zinc glycolate. Upon thermal treatment in air, this structure can be converted into a ZnO hexagonal phase with wurtzite structure via solid-state transformation. The morphology, microstructure, and crystallinity of the products before and after thermal treatment have been characterized by scanning electron microscopy, X-ray diffraction, Fourier transform infrared spectroscopy, thermogravimetric analysis, and solid-state C-13 NMR measurements. In addition, the room-temperature photoluminescence of the resulting ZnO has also been investigated.

引用

页码：3508 / 3510

页数：3

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