Analysis of saccharides in beer samples by flow injection with electrospray mass spectrometry

被引:30
作者
Mauri, P
Minoggio, M
Simonetti, P
Gardana, C
Pietta, P
机构
[1] CNR, Ist Tecnol Biomed, I-20090 Milan, Italy
[2] Dept Food Sci & Microbiol, I-20133 Milan, Italy
关键词
D O I
10.1002/rcm.632
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
Saccharides in foods play important roles, as they are essential substrates for fermentation processes. In brewing, the concentration of maltooligosaccharides influences the characteristics of beers and therefore their determination is of great practical interest. Electrospray ionization mass spectrometry (ESI-MS) was applied to identify and characterise maltooligosaccharides in beer samples. The effects due to different cation concentrations and dilution of samples were studied. Furthermore, quantitative analyses of maltooligosaccharides by means of flow-injection ESI-MS (FI/ESI-MS) of 1-muL beer samples (diluted 1000-fold) are described. Copyright (C) 2002 John Wiley Sons, Ltd.
引用
收藏
页码:743 / 748
页数:6
相关论文
共 27 条
[1]   Separation and determination of alditols and sugars by high-pH anion-exchange chromatography with pulsed amperometric detection [J].
Andersen, R ;
Sorensen, A .
JOURNAL OF CHROMATOGRAPHY A, 2000, 897 (1-2) :195-204
[2]   SEPARATION OF MONOSACCHARIDES BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY - COMPARISON OF ULTRAVIOLET AND REFRACTIVE-INDEX DETECTION [J].
BINDER, H .
JOURNAL OF CHROMATOGRAPHY, 1980, 189 (03) :414-420
[3]   Determination of sugars and alditols in food samples by HPAEC with integrated pulsed amperometric detection using alkaline eluents containing barium or strontium ions [J].
Cataldi, TRI ;
Margiotta, G ;
Zambonin, CG .
FOOD CHEMISTRY, 1998, 62 (01) :109-115
[4]   Separation of alditols of interest in food products by high-performance anion-exchange chromatography with pulsed amperometric detection [J].
Corradini, C ;
Canali, G ;
Cogliandro, E ;
Nicoletti, I .
JOURNAL OF CHROMATOGRAPHY A, 1997, 791 (1-2) :343-349
[5]  
Drawert F., 1976, Brauwissenschaft, V29, P345
[6]  
Drawert F., 1971, Brauwissenschaft, V24, P381
[7]   HPLC ANALYSIS OF CARBOHYDRATES IMPORTANT TO BEER BREWING USING AN AMINOPROPYL STATIONARY PHASE [J].
GOTSICK, JT ;
BENSON, RF .
JOURNAL OF LIQUID CHROMATOGRAPHY, 1991, 14 (10) :1887-1901
[8]   Performance and economics in micropreparative capillary electrophoresis of oligosaccharides [J].
Guttman, A ;
Sperling, E ;
Mazsaroff, I .
JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES, 1996, 19 (10) :1539-1549
[9]   Analysis of monosaccharide composition by capillary electrophoresis [J].
Guttman, A .
JOURNAL OF CHROMATOGRAPHY A, 1997, 763 (1-2) :271-277
[10]   Structural characteristics of arabinoxylan in barley, malt, and beer [J].
Han, JY .
FOOD CHEMISTRY, 2000, 70 (02) :131-138