Evaluation of size effect on mechanical properties of single crystal silicon by nanoscale bending test using AFM

被引:318
作者
Namazu, T [1 ]
Isono, Y [1 ]
Tanaka, T [1 ]
机构
[1] Ritsumeikan Univ, Fac Sci & Engn, Dept Mech Engn, Shiga 5258577, Japan
关键词
atomic force microscope (AFM); bending strength; field emission scanning electron microscope (FE-SEM); nanoscale bending test; size effect; surface roughness; Weibull parameters; Young's modulus;
D O I
10.1109/84.896765
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
This paper describes a nanometer-scale bending test for a single crustal silicon (Si) fixed beam using an atomic force microscope (AFM). This research focuses on revealing the size effect on the mechanical property of Si beams ranging from a nano- to millimeter scale, Nanometer-scale Si beams, with widths from 200 to 800 nm and a thickness of 255 nm, were fabricated on an Si diaphragm by means of field-enhanced anodization using AFM and anisotropic wet etching, The efficient condition of the held-enhanced anodization could be obtained by changing the bias voltage and the scanning speed of the cantilever. Bending tests for micro- and millimeter-scale Si beams fabricated by a photolithography technique were also carried out using an ultraprecision hardness tester and scratch tester, respectively. Comparisons of Young's modulus and bending strength of Si among the nano-, micro-, and millimeter scales showed that the specimen size did not have an influence on the Young's modulus in the [110] direction, whereas it produced a large effect on the bending strength. Observations of the fractured surface and calculations of the clack length from Griffith's theory made it clear that the maximum peak-to-valley distance of specimen surface caused the size effect on the bending strength.
引用
收藏
页码:450 / 459
页数:10
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