Towards 0.1 nm resolution with the first spherically corrected transmission electron microscope

被引:146
作者
Haider, M
Rose, H
Uhlemann, S
Kabius, B
Urban, K
机构
[1] Tech Univ Darmstadt, Inst Angew Phys, D-64289 Darmstadt, Germany
[2] CEOS GmbH, D-69120 Heidelberg, Germany
[3] Forschungszentrum Julich, Inst Festkorperforsch, D-52425 Julich, Germany
来源
JOURNAL OF ELECTRON MICROSCOPY | 1998年 / 47卷 / 05期
关键词
aberration correction; reduction of artefacts; information limit; contrast enhancement; point spread function; high-resolution TEM;
D O I
10.1093/oxfordjournals.jmicro.a023610
中图分类号
TH742 [显微镜];
学科分类号
摘要
A hexapole corrector which compensates for the spherical aberration of the objective lens has been incorporated in a commercial 200 kV transmission electron microscope (TEM) equipped with a field emission gun. The successful correction of the spherical aberration is demonstrated by decreasing the instrumental resolution limit from 0.24 nm down to about 0.13 nm. Images of Si-SiCO2 interfaces obtained with the corrected TEM show a remarkable suppression of artefacts and a strong increase in contrast apart from the improved resolution. The design, alignment and the performance of the corrected instrument are outlined in detail.
引用
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页码:395 / 405
页数:11
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