Preparation and characterization of Ba1-xSrxTiO3 (x=0.1, 0.2) fibers by sol-gel process using catechol-complexed titanium isopropoxide

被引：12

作者：

Lu, QF ^{[1
]}

Chen, DR ^{[1
]}

Jiao, XL ^{[1
]}

机构：

[1] Shandong Univ, Dept Chem, Jinan 250100, Peoples R China

来源：

JOURNAL OF ALLOYS AND COMPOUNDS | 2003年 / 358卷 / 1-2期

关键词：

chemical synthesis; nanostructures; thermal analysis; X-ray diffraction;

D O I：

10.1016/S0925-8388(03)00126-9

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Sol-gel synthesis of Ba1-xSrxTiO3 (x=0.1, 0.2) ceramic fibers with a diameter of 6-10 mum using catechol-complexed titanium isopropoxide, barium acetate hydrate and strontium acetate hydrate as precursors has been investigated. The green fibers and those sintered at different temperatures were characterized by thermogravimetry analysis (TGA), infrared spectroscopy (IR), X-ray diffraction (XRD) and scanning electron microscope (SEM) techniques. Microstructural development of barium strontium titanate (Ba1-xSrxTiO3) ceramic fibers as a function of strontium concentrations was studied. X-ray diffraction indicated that the well-developed cubic phase of (Ba, Sr)TiO3 was crystallized at 1100degreesC. (C) 2003 Elsevier B.V. All rights reserved.

引用

页码：76 / 81

页数：6

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