Comparison between two combustion routes for the synthesis of nanocrystalline SnO2 powders

被引：76

作者：

Fraigi, LB

Lamas, DG

de Reca, NEW

机构：

[1] CITEI, INTI, RA-1650 Buenos Aires, DF, Argentina

[2] UNSAM, CONICET, CITEFA, PRINSO, RA-1603 Buenos Aires, DF, Argentina

来源：

MATERIALS LETTERS | 2001年 / 47卷 / 4-5期

关键词：

SnO2; nanocrystalline powders; gel combustion process; specific surface area; crystallite size;

D O I：

10.1016/S0167-577X(00)00246-9

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Two nitrate-citrate gel combustion routes for the synthesis of nanocrystalline SnO2 powders were compared. Metallic tin and tin dichloride were used as raw materials. The combustion process was more intense for the metallic tin route, resulting in smaller crystallite size (10.5 nm) and higher specific surface area (49.4 m(2)/g). The presence of chloride ions in powders obtained by the tin dichloride route was also studied. (C) 2001 Elsevier Science B.V. All rights reserved.

引用

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页码：262 / 266

页数：5

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