Improved data acquisition in grazing-incidence X-ray scattering experiments using a pixel detector

被引:103
作者
Schlepütz, CM [1 ]
Herger, R [1 ]
Willmott, PR [1 ]
Patterson, BD [1 ]
Bunk, O [1 ]
Brönnimann, C [1 ]
Henrich, B [1 ]
Hülsen, G [1 ]
Eikenberry, EF [1 ]
机构
[1] Paul Scherrer Inst, Swiss Light Source, CH-5232 Villigen, Switzerland
来源
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES | 2005年 / 61卷
关键词
D O I
10.1107/S0108767305014790
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The use of an area detector in grazing-incidence X-ray experiments lends many advantages in terms of both speed and reliability. Here a discussion is given of the procedures established using the PILATUS pixel detector developed at the Swiss Light Source for optimizing data acquisition and analysis of surface diffraction data at the Materials Science beamline, especially with regard to reflectivity measurements, crystal truncation and fractional order rods, and grazing-incidence diffraction experiments.
引用
收藏
页码:418 / 425
页数:8
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