A simple solvothermal synthesis and characterization of round-biscuit-like Fe3O4 nanoparticles with adjustable sizes

被引：34

作者：

Yan, Aiguo

Liu, Xiaohe ^{[1
]}

Qiu, Guanzhou

Zhang, Ning

Shi, Rongrong

Yi, Ran

Tang, Motang

Che, Renchao

机构：

[1] Cent S Univ, Dept Inorgan Mat, Changsha 410083, Peoples R China

[2] Cent S Univ, Sch Met Sci & Engn, Changsha 410083, Peoples R China

[3] Natl Univ Defense Technol, Sch Aerosp & Mat Engn, Changsha 410073, Peoples R China

来源：

SOLID STATE COMMUNICATIONS | 2007年 / 144卷 / 7-8期

基金：

中国博士后科学基金; 中国国家自然科学基金;

关键词：

nanostructures; magnetic materials; chemical synthesis;

D O I：

10.1016/j.ssc.2007.08.039

中图分类号：

O469 [凝聚态物理学];

学科分类号：

070205 ;

摘要：

Round-biscuit-like Fe3O4 nanoparticles were successfully prepared in large-scale by a simple solvothermal method. The sizes of the particles can be readily tuned from 15 to 150 run by adjusting the experimental parameters such as solvothermal temperature, reaction time, the initial concentration of the reactants, and molar ratio of FeCl3 and protective reagents. Structure, morphology and size products were investigated in detail by X-ray diffraction (XRD), transmission electron microscopy (TEM), selected area electron diffraction (SAED) and scanning electron microscopy (SEM). Magnetic studies revealed that the saturation magnetization (M,) increases as the particle size increases. (c) 2007 Elsevier Ltd. All rights reserved.

引用

页码：315 / 318

页数：4

共 31 条

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