Porous network of Y2O3 nanorods prepared by electrogeneration of base in chloride medium

被引：58

作者：

Aghazadeh, Mustafa ^{[1
,2
]}

Ghaemi, Mehdi ^{[3
]}

Golikand, Ahmad Nozad ^{[1
]}

Ahmadi, Ali ^{[1
]}

机构：

[1] NSTRI, Mat Res Sch, Tehran, Iran

[2] Tarbiat Modares Univ, Dept Chem, Tehran, Iran

[3] Golestan Univ, Fac Sci, Dept Chem, Gorgan, Iran

来源：

MATERIALS LETTERS | 2011年 / 65卷 / 15-16期

关键词：

Electrodeposition; Y(OH)(3); Y2O3; Nanorods; Thermal analysis; YSZ THIN-FILMS; ELECTROCHEMICAL SYNTHESIS; DEPOSITION; Y(OH)(3); YTTRIA; OXIDE;

D O I：

10.1016/j.matlet.2011.02.044

中图分类号：

T [工业技术];

学科分类号：

120111 [工业工程];

摘要：

A porous network of Y2O3 nanorods was successfully prepared by an easy two-step and template-free process. Firstly, Y(OH)(3) was galvanostatically grown on steel cathode by electrogeneration of base in chloride medium. Then it was thermally converted to oxide via heat treatment. Phase transformations during the heat treatment of deposit were proposed. Morphological studies showed that the obtained oxide has a porous network, composed of intercrossed nanorods. The nanorods are 200-300 nm in length and 50-70 nm in diameter. The mechanism of base electrogeneration in chloride medium, the deposition of Y(OH)(3) nanorods on the cathode surface and their thermal conversion to Y2O3 have been discussed. (C) 2011 Elsevier B.V. All rights reserved.

引用

页码：2545 / 2548

页数：4

共 16 条

[1]

Synthesis of Y2O3 Nanospheres via Heat-Treatment of Cathodically Grown Y(OH)3 in Chloride Medium [J].