Synthesis of molybdenum (IV) disulfide using a single-source method

被引：11

作者：

Monteiro, OC ^{[1
]}

Trindade, T ^{[1
]}

机构：

[1] Univ Aveiro, Dept Chem, CICECO, P-3810193 Aveiro, Portugal

来源：

MATERIALS RESEARCH BULLETIN | 2004年 / 39卷 / 03期

关键词：

metal sulfides; chemical synthesis; microstructure;

D O I：

10.1016/j.materresbull.2003.11.001

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Molybdenum(IV) disulfide was prepared by the thermalysis of the single molecule precursor [Mo2O4(S2C- NEt2)(2)] (Et: ethyl group). The thermalysis was monitored by thermogravimetric analysis and FT-infrared spectroscopy. The MoS2 materials obtained during the thermalysis experiments were characterized in terms of their morphological and optical characteristics. (C) 2003 Elsevier Ltd. All rights reserved.

引用

页码：357 / 363

页数：7

共 20 条

[1]

Burdett J. K., 1995, CHEM BONDING SOLIDS

[2] Bulk synthesis of inorganic fullerene-like MS(2) (M=Mo, W) from the respective trioxides and the reaction mechanism [J].

Feldman, Y ;

Frey, GL ;

Homyonfer, M ;

Lyakhovitskaya, V ;

Margulis, L ;

Cohen, H ;

Hodes, G ;

Hutchison, JL ;

Tenne, R .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1996, 118 (23) :5362-5367

[3]

Monteiro OC, 2000, CHEM VAPOR DEPOS, V6, P230, DOI 10.1002/1521-3862(200010)6:5<230::AID-CVDE230>3.0.CO

[4]

2-P

[5] Use of dialkyldithiocarbamato complexes of bismuth(III) for the preparation of nano- and microsized Bi2S3 particles and the X-ray crystal structures of [Bi{S2CN(CH3)(C6H13)}3] and [Bi{S2CN(CH3)(C6H13)}3(C12H8N2)] [J].

Monteiro, OC ;

Nogueira, HIS ;

Trindade, T ;

Motevalli, M .

CHEMISTRY OF MATERIALS, 2001, 13 (06) :2103-2111

[6] Synthesis, characterization and X-ray crystal structures of asymmetric bis(dialkyldithiocarbamates) of zinc: Potential precursors for ZnS deposition [J].

Motevalli, M ;

OBrien, P ;

Walsh, JR ;

Watson, IM .

POLYHEDRON, 1996, 15 (16) :2801-2808

[7]

Nath M, 2001, ADV MATER, V13, P283, DOI 10.1002/1521-4095(200102)13:4<283::AID-ADMA283>3.0.CO

[8]

2-H

[9]

OKAMOTO Y, 1996, J CHEM SOC FARADAY T, V92, P4656

[10] Electrochemical deposition of MoS2 thin films by reduction of tetrathiomolybdate [J].

Ponomarev, EA ;

NeumannSpallart, M ;

Hodes, G ;

LevyClement, C .

THIN SOLID FILMS, 1996, 280 (1-2) :86-89

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