Synthesis and characterization of single-wall carbon nanotubes by hot-filament assisted chemical vapor deposition

被引:32
作者
Okazaki, T
Shinohara, H [1 ]
机构
[1] Nagoya Univ, Dept Chem, Nagoya, Aichi 4648602, Japan
[2] Nagoya Univ, Inst Adv Res, Nagoya, Aichi 4648602, Japan
[3] Nagoya Univ, CREST, Japan Sci Technol Corp, Dept Chem, Nagoya, Aichi 4648602, Japan
关键词
D O I
10.1016/S0009-2614(03)01042-X
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
We report a simplified production method for single-wall carbon nanotubes (SWNTs) by hot-filament assisted chemical vapor deposition (HFCVD) using pure alcohol vapor (ethanol, methanol and 2-propanol) as a carbon source. Under the optimized conditions, high-purity SWNTs are synthesized for the first time in large quantities. Raman spectra of the synthesized SWNTs show similar G/D ratios and the peak distribution of radial breathing mode to those obtained by the conventional CVD method with an electric furnace. The efficiency of the SWNTs synthesis has been increased by the hot-filament-induced pyrolysis of carbon sources, which promises an easy scale-up of the production of SWNTs at a low cost. (C) 2003 Elsevier B.V. All rights reserved.
引用
收藏
页码:606 / 611
页数:6
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