Multiple-wavelength powder diffraction using imaging plates at the Australian National Beamline

被引:6
作者
Cookson, DJ [1 ]
Hunter, BA [1 ]
Kennedy, SJ [1 ]
Garrett, RF [1 ]
机构
[1] Australian Nucl Sci & Technol Org, Menai, NSW 2234, Australia
关键词
imaging plates; X-ray powder diffraction; anomalous scattering; high-T-c superconductors;
D O I
10.1107/S0909049597016634
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
The Australian powder diffractometer at the Photon Factory is capable of recording multiple powder-diffraction scans in less than 5 min per pattern using imaging plates in Debye-Scherrer geometry. This, coupled with incrementing the X-ray beam energy in suitably small steps (down to similar to 2eV) between exposures, allows fast collection of anomalous diffraction data. Data collected from a copper oxide-based superconductor at energies near the Cu K-absorption edge are presented, along with an account of the technique used to extract multiple-exposure powder-diffraction data from imaging plates.
引用
收藏
页码:926 / 928
页数:3
相关论文
共 14 条
[1]   DESIGN AND PERFORMANCE OF AN IMAGING PLATE SYSTEM FOR X-RAY-DIFFRACTION STUDY [J].
AMEMIYA, Y ;
MATSUSHITA, T ;
NAKAGAWA, A ;
SATOW, Y ;
MIYAHARA, J ;
CHIKAWA, J .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 1988, 266 (1-3) :645-653
[2]   RESONANT POWDER X-RAY-DIFFRACTION APPLIED TO MIXED-VALENCE COMPOUNDS AND THE POSSIBILITY OF SITE-RESOLVED X-RAY ABSORPTION-SPECTROSCOPY ILLUSTRATED FOR YBA2CU3O6.27 [J].
ATTFIELD, JP .
JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 1991, 52 (10) :1243-1249
[3]   DETERMINATION OF VALENCE AND CATION DISTRIBUTIONS BY RESONANT POWDER X-RAY-DIFFRACTION [J].
ATTFIELD, JP .
NATURE, 1990, 343 (6253) :46-49
[4]   THE AUSTRALIAN DIFFRACTOMETER AT THE PHOTON FACTORY [J].
BARNEA, Z ;
CREAGH, DC ;
DAVIS, TJ ;
GARRETT, RF ;
JANKY, S ;
STEVENSON, AW ;
WILKINS, SW .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1992, 63 (01) :1069-1072
[5]   Refinement of powder diffraction data collected using imaging plates [J].
Cookson, DJ ;
Foran, GJ ;
Hunter, BA ;
Ismunandar ;
Kennedy, BJ .
EUROPEAN POWDER DIFFRACTION: EPDIC IV, PTS 1 AND 2, 1996, 228 :113-118
[6]   X-Ray diffraction from layers of n-alkanes adsorbed on graphite [J].
Espeau, P ;
Reynolds, PA ;
Dowling, T ;
Cookson, D ;
White, JW .
JOURNAL OF THE CHEMICAL SOCIETY-FARADAY TRANSACTIONS, 1997, 93 (17) :3201-3208
[7]   POWDER DIFFRACTION USING IMAGING PLATES AT THE AUSTRALIAN NATIONAL BEAMLINE FACILITY AT THE PHOTON FACTORY [J].
GARRETT, RF ;
COOKSON, DJ ;
FORAN, GJ ;
SABINE, TM ;
KENNEDY, BJ ;
WILKINS, SW .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1995, 66 (02) :1351-1353
[8]   Influence of solution constituents, solution conditioning and seeding on the crystalline phase of aluminium hydroxide using in situ X-ray diffraction [J].
Gerson, AR ;
Counter, JA ;
Cookson, DJ .
JOURNAL OF CRYSTAL GROWTH, 1996, 160 (3-4) :346-354
[9]  
HILL RJ, 1986, M112 AUSTR NUCL SCI
[10]  
HUNTER BA, 1997, UNPUB