Modern diffusion-ordered NMR spectroscopy in chemistry of supramolecular systems: the scope and limitations

被引：38

作者：

Kharlamov, S. V. ^{[1
]}

Latypov, Sh K. ^{[1
]}

机构：

[1] Russian Acad Sci, Kazan Res Ctr, AE Arbuzov Organ & Phys Chem Inst, Kazan 420088, Russia

来源：

RUSSIAN CHEMICAL REVIEWS | 2010年 / 79卷 / 08期

基金：

俄罗斯基础研究基金会;

关键词：

NUCLEAR-MAGNETIC-RESONANCE; GRADIENT SPIN-ECHO; HIGH-RESOLUTION DIFFUSION; STUDYING TRANSLATIONAL DIFFUSION; EDDY-CURRENT COMPENSATION; CHEMICAL-MIXTURE ANALYSIS; MOLECULAR-MASS ESTIMATION; RANK ANNIHILATION METHOD; PULSED-FIELD GRADIENTS; AMIDE PROTON-EXCHANGE;

D O I：

10.1070/RC2010v079n08ABEH004148

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The concept of diffusion-ordered NMR spectroscopy (self-diffusion coefficients measurement in high-resolution mode) is considered. The most important aspects of interpretation of experimental data, as well as the scope and limitations of the available theoretical and phenomenological models relating the self-diffusion coefficient to the size or mass of the molecular system are discussed.

引用

页码：635 / 653

页数：19

共 225 条

[1] Discrimination of metallosupramolecular architectures in solution by using diffusion ordered spectroscopy (DOSY) experiments: Double-stranded helicates of different lengths [J].

Allouche, Lionel ;

Marquis, Annie ;

Lehnl, Jean-Marie .

CHEMISTRY-A EUROPEAN JOURNAL, 2006, 12 (28) :7520-7525

[2]

Ananikov V. P., 2009, Russian Nanotechnologies, V4, P56

[3]

ANANIKOV VP, 2008, IZV AKAD NAUK K, P740

[4]

[Anonymous], 1989, NUCL OVERHAUSER EFFE, DOI DOI 10.1002/MRC.1260280819

[5]

[Anonymous], 1990, Principles of Nuclear Magnetic Resonance in One and Two Dimensions

[6] Using pulsed gradient spin echo NMR for chemical mixture analysis: How to obtain optimum results [J].

Antalek, B .

CONCEPTS IN MAGNETIC RESONANCE, 2002, 14 (04) :225-258

[7] Generalized rank annihilation method applied to a single multicomponent pulsed gradient spin echo NMR data set [J].

Antalek, B ;

Windig, W .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1996, 118 (42) :10331-10332

[8] Using PGSE NMR for chemical mixture analysis: Quantitative aspects [J].

Antalek, Brian .

CONCEPTS IN MAGNETIC RESONANCE PART A, 2007, 30A (05) :219-235

[9]

ATTAURRAHMAN, 1989, 1 2 DIMENSIONAL NMR

[10] NMR Measure of Translational Diffusion and Fractal Dimension. Application to Molecular Mass Measurement [J].

Auge, Sophie ;

Schmit, Pierre-Olivier ;

Crutchfield, Christopher A. ;

Islam, Mohammad T. ;

Harris, Douglas J. ;

Durand, Emmanuelle ;

Clemancey, Martin ;

Quoineaud, Anne-Agathe ;

Lancelin, Jean-Marc ;

Prigent, Yann ;

Taulelle, Francis ;

Delsuc, Marc-Andre .

JOURNAL OF PHYSICAL CHEMISTRY B, 2009, 113 (07) :1914-1918

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