Preparation of Bi2S3 nanorods by microwave irradiation

被引：132

作者：

Liao, XH

Wang, H

Zhu, JJ ^{[1
]}

Chen, HY

机构：

[1] Nanjing Univ, State Key Lab Coordinat Chem, Dept Chem, Nanjing 210093, Peoples R China

[2] Huazhong Normal Univ, Huangzhou 438000, Hubei, Peoples R China

来源：

MATERIALS RESEARCH BULLETIN | 2001年 / 36卷 / 13-14期

基金：

国家教育部科学基金资助; 中国国家自然科学基金;

关键词：

semiconductors; nanostructures; chemical synthesis; X-ray diffraction;

D O I：

10.1016/S0025-5408(01)00734-6

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Bi2S3 nanorods, with a diameter of ca. 10 nm and a length of up to ca. 300 nm, have been successfully prepared from a formaldehyde solution of bismuth nitrate and thiourea by microwave irradiation. Powder X-ray diffraction (XRD) pattern indicates that the product is pure orthorhombic Bi2S3 phase. The product is also characterized by the techniques of transmission electron microscopy (TEM) and X-ray photoelectron spectra (XPS). (C) 2001 Elsevier Science Ltd. All rights reserved.

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收藏

页码：2339 / 2346

页数：8

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