A modified Pinkerton-type helium gas-flow system for high-accuracy data collection at the X3 SUNY synchrotron beamline at NSLS

被引:30
作者
Ribaud, L [1 ]
Wu, G [1 ]
Zhang, YG [1 ]
Coppens, P [1 ]
机构
[1] SUNY Buffalo, Dept Chem, Buffalo, NY 14260 USA
关键词
D O I
10.1107/S0021889800014291
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
As the combination of high-intensity synchrotron sources and area detectors allows collection of large data sets in a much shorter time span than previously possible, the use of open helium gas-flow systems is much facilitated. A flow system installed at the SUNY X3 synchrotron beamline at the National Synchrotron Light Source has been used for collection of a number of large data sets at a temperature of similar to 16 K. Instability problems encountered when using a helium cryostat for three-dimensional data collection are eliminated. Details of the equipment, its temperature calibration and a typical result are described.
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页码:76 / 79
页数:4
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