Determination of salbutamol and detection of other β-agonists in human postmortem whole blood and urine by GC-MS-SIM

被引:19
作者
Black, SB [1 ]
Hansson, RC [1 ]
机构
[1] Chem Ctr WA, Forens Sci Lab, E Perth, WA 6004, Australia
关键词
D O I
10.1093/jat/23.2.113
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
This paper details a sensitive and quantitative method for the determination of salbutamol and the detection of terbutaline, clenbuterol, fenoterol, and isoprenaline in postmortem human whole blood and urine. It describes solid-phase extraction using a XtrackT XRDAH515 column, formation of trimethylsilyl derivatives, and analysis by gas chromatography-mass spectrometry-selective ion monitoring.
引用
收藏
页码:113 / 118
页数:6
相关论文
共 34 条
[11]   OPTIMIZATION OF A COLUMN LIQUID-CHROMATOGRAPHIC PROCEDURE FOR THE DETERMINATION OF PLASMA SALBUTAMOL CONCENTRATION [J].
GUPTA, RN ;
FULLER, HD ;
DOLOVICH, MB .
JOURNAL OF CHROMATOGRAPHY B-BIOMEDICAL APPLICATIONS, 1994, 654 (02) :205-211
[12]   DETERMINATION OF SALBUTAMOL IN PLASMA BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY WITH FLUORESCENCE DETECTION [J].
HUTCHINGS, MJ ;
PAULL, JD ;
MORGAN, DJ .
JOURNAL OF CHROMATOGRAPHY, 1983, 277 (OCT) :423-426
[13]   REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC DETERMINATION OF SALBUTAMOL IN RABBIT PLASMA [J].
KUROSAWA, N ;
MORISHIMA, S ;
OWADA, E ;
ITO, K .
JOURNAL OF CHROMATOGRAPHY, 1984, 305 (02) :485-488
[14]   QUANTITATIVE-ANALYSIS OF TERBUTALINE IN SERUM AND URINE AT THERAPEUTIC LEVELS USING GAS CHROMATOGRAPHY MASS SPECTROMETRY [J].
LEFERINK, JG ;
WAGEMAKERENGELS, I ;
MAES, RAA ;
LAMONT, H ;
PAUWELS, R ;
VANDERSTRAETEN, M .
JOURNAL OF CHROMATOGRAPHY, 1977, 143 (03) :299-305
[15]   A TIME-SAVING METHOD FOR THE DETERMINATION OF THE BETA-2 SYMPATHOMIMETICS TERBUTALINE, SALBUTAMOL AND FENOTEROL - PRELIMINARY-RESULTS [J].
LEFERINK, JG ;
DANKERS, J ;
MAES, RAA .
JOURNAL OF CHROMATOGRAPHY, 1982, 229 (01) :217-221
[16]  
LEFERINK JG, 1979, VET HUM TOXICOL, V21, P164
[17]   EVALUATION OF A HIGH-PERFORMANCE THIN-LAYER CHROMATOGRAPHIC TECHNIQUE FOR THE DETERMINATION OF SALBUTAMOL SERUM LEVELS IN CLINICAL-TRIALS [J].
LEROUX, AM ;
WIUM, CA ;
JOUBERT, JR ;
VANJAARSVELD, PP .
JOURNAL OF CHROMATOGRAPHY-BIOMEDICAL APPLICATIONS, 1992, 581 (02) :306-309
[18]   DETERMINATION OF BETA-2-RECEPTOR AGONISTS IN BOVINE URINE AND LIVER BY GAS-CHROMATOGRAPHY TANDEM MASS-SPECTROMETRY [J].
LEYSSENS, L ;
DRIESSEN, C ;
JACOBS, A ;
CZECH, J ;
RAUS, J .
JOURNAL OF CHROMATOGRAPHY-BIOMEDICAL APPLICATIONS, 1991, 564 (02) :515-527
[19]   SIMULTANEOUS DETERMINATION OF TERBUTALINE AND SALBUTAMOL IN PLASMA BY SELECTED ION MONITORING [J].
LINDBERG, C ;
JONSSON, S .
BIOMEDICAL MASS SPECTROMETRY, 1982, 9 (11) :493-494
[20]  
LOO JCK, 1987, RES COMMUN CHEM PATH, V55, P282