Preparation of CdS and ZnS nanoparticles using microwave irradiation

被引:154
作者
Zhu, JJ [1 ]
Zhou, MG [1 ]
Xu, JZ [1 ]
Liao, XH [1 ]
机构
[1] Nanjing Univ, Dept Chem, State Key Lab Coordinat Chem, Nanjing 210093, Peoples R China
关键词
microwave irradiation; nanoparticles; CdS; ZnS; preparation; characterization;
D O I
10.1016/S0167-577X(00)00206-8
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Nanoparticles of CdS, ZnS have been prepared by a very simple fast reaction between CdCl2 or Zn(Ac)(2) and thioacetamide in aqueous solution using microwave irradiation. The nanoparticles were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), reflectance and photoluminescence spectra. The sizes of the sample as prepared were calculated by Debye-Scherrer formula according to XRD spectra to be about 9 and 3 nm for CdS and ZnS, respectively. Similar results can also been obtained in the TEM images. (C) 2001 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:25 / 29
页数:5
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