Synthesis of highly ordered CdSe nanowire arrays embedded in anodic alumina membrane by electrodeposition in ammonia alkaline solution

被引:84
作者
Peng, XS [1 ]
Zhang, J [1 ]
Wang, XF [1 ]
Wang, YW [1 ]
Zhao, LX [1 ]
Meng, GW [1 ]
Zhang, LD [1 ]
机构
[1] Chinese Acad Sci, Inst Solid State Phys, Hefei 230031, Peoples R China
基金
中国国家自然科学基金;
关键词
D O I
10.1016/S0009-2614(01)00722-9
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Highly ordered polycrystalline CdSe nanowire arrays have been synthesized by direct current (dc) electrodeposition in anodic alumina membrane (AAM) from ammonia alkaline solution containing CdCl2 and SeO2. These nanowires have uniform diameters of about 60 nm, which correspond to the pore sizes of the membranes used. The X-ray diffraction (XRD) patterns indicate that the CdSe nanowires crystallize in a wurtzite structure. The X-ray photoelectron energy spectroscopy and the energy dispersing analysis spectroscopy investigations demonstrate that stoichiometric CdSe is formed, and the ratio of selenium to cadmium depends on the pH of the deposition bath. A mechanism for the nanowires growth is suggested. (C) 2001 Elsevier Science BN. All rights reserved.
引用
收藏
页码:470 / 474
页数:5
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