X-ray absolute intensity measurement at HASYLAB ultrasmall angle x-ray scattering beamline BW4

被引：11

作者：

Endres, A ^{[1
]}

Lode, U ^{[1
]}

vonKrosigk, G ^{[1
]}

Bark, M ^{[1
]}

Cunis, S ^{[1
]}

Gehrke, R ^{[1
]}

Wilke, W ^{[1
]}

机构：

[1] DESY,HASYLAB,D-22603 HAMBURG,GERMANY

来源：

REVIEW OF SCIENTIFIC INSTRUMENTS | 1997年 / 68卷 / 11期

关键词：

D O I：

10.1063/1.1148374

中图分类号：

TH7 [仪器、仪表];

学科分类号：

0804 ; 080401 ; 081102 ;

摘要：

In order to obtain small angle scattering intensities in absolute units, measurements of the incident beam intensity and the intensity transmitted through the sample are required. For this purpose the scattering intensity of a calibrated polyethylene (LUPOLEN) standard is used. For the determination of the absolute photon flux and the correction of the scattering patterns obtained with a two dimensional position sensitive detector we use the detector response function. A set of data measured subsequently at the standard and at a given sample can be evaluated in a program that calculates a pattern in absolute units corrected by means of the detector response. This program also calculates the absolute photon flux, determines automatically the center coordinates of the incident beam, and calculates the scattering vectors that belong to the different positions on the detector. (C) 1997 American Institute of Physics. [S0034-6748(97)02111-4].

引用

页码：4009 / 4013

页数：5

共 14 条

[1] THE LOCALIZATION METHOD USED AT EMBL [J].