2,2,4,4,6,6-Hexabenzylcyclotristannatellurane (Bn2SnTe)3.: Synthesis and structural characterization of an organometallic single-source precursor to phase-pure, polycrystalline SnTe

被引:32
作者
Boudjouk, P [1 ]
Remington, MP [1 ]
Grier, DG [1 ]
Triebold, W [1 ]
Jarabek, BR [1 ]
机构
[1] N Dakota State Univ, Ctr Main Grp Chem, Dept Chem, Fargo, ND 58105 USA
关键词
D O I
10.1021/om990506u
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
The title compound, (Bn2SnTe)(3) Bn = CH2CsH5, was prepared in high yield by treating Bn2SnCl2 with (NH4)(2)Te. Details of the synthesis and characterization (H-1, C-13, Sn-119, and Te-125 NMR; IR, single-crystal XRD, and elemental analyses) are presented. (Bn2SnTe)(3) serves as an efficient single-source precursor to phase-pure cubic SnTe under mild conditions.
引用
收藏
页码:4534 / 4537
页数:4
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