Preparation and characterization of SnO nanowhiskers

被引:43
作者
Jia, ZJ
Zhu, LP [1 ]
Liao, GH
Yu, Y
Tang, YW
机构
[1] Cent China Normal Univ, Dept Phys, Ctr Nanosci & Technol, Wuhan 430079, Peoples R China
[2] Cent China Normal Univ, Coll Chem, Wuhan 430079, Peoples R China
关键词
nanostructures; semiconductors; chemical synthesis;
D O I
10.1016/j.ssc.2004.07.028
中图分类号
O469 [凝聚态物理学];
学科分类号
070205 ;
摘要
In this paper, some single-crystal line Stannous oxide (SnO) nanowhiskers were successfully prepared by a wet method using SnCl2 . 2H(2)O as raw material and cetyltrimethylammoniumbromide (CTAB) as surfactant. The morphologies, purity and sizes of the products were characterized by transmission electron microscopy, powder X-ray diffractmetry and standard selected area electron diffraction. The results showed that the diameter and the length of the particles were 10-30 and 200-400 nm, respectively. The influence of some reaction parameters, including the pressure, the temperature, the surfactant and the reaction duration, on the formation, morphology and particle size of SnO crystallite is discussed. (C) 2004 Elsevier Ltd. All rights reserved.
引用
收藏
页码:79 / 82
页数:4
相关论文
共 13 条
[1]   Semiconductor clusters, nanocrystals, and quantum dots [J].
Alivisatos, AP .
SCIENCE, 1996, 271 (5251) :933-937
[2]  
DAI H, 1999, NATURE, V375, P769
[3]   Carbon nanotube quantum resistors [J].
Frank, S ;
Poncharal, P ;
Wang, ZL ;
de Heer, WA .
SCIENCE, 1998, 280 (5370) :1744-1746
[4]   Preparation of Bi2S3 nanowhiskers and their morphologies [J].
He, R ;
Qian, XF ;
Yin, J ;
Zhu, ZK .
JOURNAL OF CRYSTAL GROWTH, 2003, 252 (04) :505-510
[5]   Nanoscale materials [J].
Heath, JR .
ACCOUNTS OF CHEMICAL RESEARCH, 1999, 32 (05) :388-388
[6]   Growth and morphologies of large-scale SnO2 nanowires, nanobelts and nanodendrites [J].
Jian, JK ;
Chen, XL ;
Wang, WJ ;
Dai, L ;
Xu, YP .
APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING, 2003, 76 (02) :291-294
[7]   OBSERVATION OF QUANTUM EFFECTS AND COULOMB-BLOCKADE IN SILICON QUANTUM-DOT TRANSISTORS AT TEMPERATURES OVER 100 K [J].
LEOBANDUNG, E ;
GUO, LJ ;
WANG, Y ;
CHOU, SY .
APPLIED PHYSICS LETTERS, 1995, 67 (07) :938-940
[8]   A high-rate, high-capacity, nanostructured Sn-based anode prepared using sol-gel template synthesis [J].
Li, NC ;
Martin, CR .
JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 2001, 148 (02) :A164-A170
[9]   Mechanism of the electrochemical insertion of lithium into LiMn2O4 spinels [J].
Liu, W ;
Kowal, K ;
Farrington, GC .
JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 1998, 145 (02) :459-465
[10]   Active/inactive nanocomposites as anodes for Li-ion batteries [J].
Mao, O ;
Turner, RL ;
Courtney, IA ;
Fredericksen, BD ;
Buckett, MI ;
Krause, LJ ;
Dahn, JR .
ELECTROCHEMICAL AND SOLID STATE LETTERS, 1999, 2 (01) :3-5