Extraction, separation and identification of volatile organic compounds from paprika oleoresin (Spanish type)

被引:34
作者
Guadayol, JM [1 ]
Caixach, J [1 ]
Ribe, J [1 ]
Cabanas, J [1 ]
Rivera, J [1 ]
机构
[1] CSIC,CID,LAB ESPECTROMETRIA MASSES,ES-08034 BARCELONA,SPAIN
关键词
paprika oleoresin; simultaneous distillation-extraction (SDE); dynamic headspace; purge and trap; static headspace; HRGC-MS; VOCs; Capsicum annuum;
D O I
10.1021/jf960266i
中图分类号
S [农业科学];
学科分类号
09 ;
摘要
In the present work the extraction, separation, identification, and quantification ofVOCs in paprika oleoresin were performed. Five different methods were used for extraction: simultaneous distillation-extraction (SDE) at atmospheric and reduced pressures, static and dynamic headspace, and purge and trap. The results obtained were compared and assessed. Separation, identification, and quantification were carried out by HRGC-FID and HRGC-MS. Samples of red pepper from Murcia (Spain) were obtained by industrial extraction. Ail treated samples are manufactured as paprika oleoresin to be used as a colorant. The VOCs identified in paprika oleoresin, which have also been found in other foods, are reported.
引用
收藏
页码:1868 / 1872
页数:5
相关论文
共 19 条
[1]   TRENDS IN PURGE-AND-TRAP [J].
ABEEL, SM ;
VICKERS, AK ;
DECKER, D .
JOURNAL OF CHROMATOGRAPHIC SCIENCE, 1994, 32 (08) :328-338
[2]  
BUTTERY RG, 1993, ACS SYM SER, V525, P23
[3]  
CABEZA A, 1992, FOOD PROCESSING IND, V1, P351
[4]   GC MS AND SENSORY ANALYSIS OF VOLATILES FROM 3 CULTIVARS OF CAPSICUM [J].
CHITWOOD, RL ;
PANGBORN, RM ;
JENNINGS, W .
FOOD CHEMISTRY, 1983, 11 (03) :201-216
[5]  
COLE A, 1992, LC GC INT, V3, P8
[6]   CAPSICUM - PRODUCTION, TECHNOLOGY, CHEMISTRY, AND QUALITY .3. CHEMISTRY OF THE COLOR, AROMA, AND PUNGENCY STIMULI [J].
GOVINDARAJAN, VS .
CRC CRITICAL REVIEWS IN FOOD SCIENCE AND NUTRITION, 1986, 24 (03) :245-355
[7]   SEPARATION AND ISOLATION OF VOLATILE ORGANIC-COMPOUNDS USING VACUUM DISTILLATION WITH GC/MS DETERMINATION [J].
HIATT, MH ;
YOUNGMAN, DR ;
DONNELLY, JR .
ANALYTICAL CHEMISTRY, 1994, 66 (06) :905-908
[8]  
Keller U., 1981, ACS Symposium Series, V170, P137
[9]  
LIKENS ST, 1964, AM SOC BREWING CHEM, P5
[10]  
MAARSE H, 1989, VOLATILE COMPOUND S1, V2