Synthesis and characterization of nanophasic LaCoO3 powders

被引：46

作者：

Armelao, L

Bandoli, G

Barreca, D

Bettinelli, M

Bottaro, G

Caneschi, A

机构：

[1] Univ Padua, ISTM, CNR, I-35131 Padua, Italy

[2] Univ Padua, INSTM, Dipartimento CIMA, I-35131 Padua, Italy

[3] Univ Padua, Dipartimento Sci Farmaceut, I-35131 Padua, Italy

[4] Univ Verona, Dipartimento Sci & Tecnol, I-37100 Verona, Italy

[5] Univ Florence, Dipartimento Chim, Florence, Italy

[6] Univ Florence, INSTM, Florence, Italy

来源：

SURFACE AND INTERFACE ANALYSIS | 2002年 / 34卷 / 01期

关键词：

lanthanum cobaltite; nanopowders; XPS; EPR; XRD;

D O I：

10.1002/sia.1264

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Nanophasic LaCoO3 powders were synthesized from inorganic compounds both in molten chloride fluxes and by using a solution combustion synthesis procedure. The samples were prepared in air and underwent subsequent heat treatments in order to yield the perovskite crystalline phase. The composition and microstructure of the samples were investigated by XPS, x-ray-induced AES, x-ray diffraction and electron paramagnetic resonance. Further information was gained by magnetic measurements. Nanophasic LaCoO3 powders with an average crystallite size of 35 nm were obtained. Copyright (C) 2002 John Wiley Sons, Ltd.

引用

页码：112 / 115

页数：4

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