Determination of the enantiomeric ratio of unprotected amino acids by NMR spectroscopy with C-2-chiral palladium compounds

被引：42

作者：

Staubach, B ^{[1
]}

Buddrus, J ^{[1
]}

机构：

[1] UNIV DORTMUND, INST SPEKTROCHEM & ANGEW SPEKTROSKOPIE, D-44013 DORTMUND, GERMANY

来源：

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION | 1996年 / 35卷 / 12期

关键词：

amino acids; chiral auxiliaries; NMR spectroscopy; palladium compounds;

D O I：

10.1002/anie.199613441

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

[No abstract available]

引用

页码：1344 / 1346

页数：3

共 32 条

[11] ASYMMETRIC-SYNTHESIS OF NEW CHIRAL EUROPIUM N,N'-DISUCCINATE COMPLEXES - SHIFT-REAGENTS FOR AQUEOUS-SOLUTIONS AND APPLICATION IN THE ENANTIOMERIC EXCESS DETERMINATION OF AMINO-ACIDS [J].

HULST, R ;

DEVRIES, NK ;

FERINGA, BL .

JOURNAL OF ORGANIC CHEMISTRY, 1994, 59 (24) :7453-7458

[12]

HULST R, 1995, RECL TRAV CHIM PAY B, V114, P115

[13]

HULST R, 1992, ANGEW CHEM INT EDIT, V31, P1092, DOI 10.1002/anie.199210921

[14] (S)-2H-2-OXO-5,5-DIMETHYL-4(R)-PHENYL-1,3,2-DIOXAPHOSPHORINANE, A NEW REAGENT FOR THE ENANTIOMERIC EXCESS DETERMINATION OF UNPROTECTED AMINO-ACIDS USING P-31 NMR [J].

HULST, R ;

ZIJLSTRA, RWJ ;

DEVRIES, NK ;

FERINGA, BL .

TETRAHEDRON-ASYMMETRY, 1994, 5 (09) :1701-1710

[15]

Hulst R., 1992, ANGEW CHEM, V104, P1089

[16] SEPARATION AND DETECTION OF AMINO-ACIDS AND THEIR ENANTIOMERS BY CAPILLARY ELECTROPHORESIS - A REVIEW [J].

ISSAQ, HJ ;

CHAN, KC .

ELECTROPHORESIS, 1995, 16 (04) :467-480

[17] THE EUROPIUM(III) (R)-PROPYLENEDIAMINETETRA-ACETATE ION - A PROMISING CHIRAL SHIFT-REAGENT FOR H-1-NMR SPECTROSCOPY IN AQUEOUS-SOLUTION [J].

KABUTO, K ;

SASAKI, Y .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1984, (05) :316-318

[18] EUROPIUM (S,S)-ETHYLENEDIAMINE-N,N'-DISUCCINATE AS A CHIRAL LANTHANIDE SHIFT-REAGENT FOR AQUEOUS-SOLUTIONS [J].

KIDO, J ;

OKAMOTO, Y ;

BRITTAIN, HG .

JOURNAL OF ORGANIC CHEMISTRY, 1991, 56 (04) :1412-1415

[19] SYNTHESIS OF OPTICALLY PURE ALPHA-ALKYLATED ALPHA-AMINO-ACIDS AND A SINGLE-STEP METHOD FOR ENANTIOMERIC EXCESS DETERMINATION [J].

KRUIZINGA, WH ;

BOLSTER, J ;

KELLOGG, RM ;

KAMPHUIS, J ;

BOESTEN, WHJ ;

MEIJER, EM ;

SCHOEMAKER, HE .

JOURNAL OF ORGANIC CHEMISTRY, 1988, 53 (08) :1826-1827

[20] NATURE OF CIS AMINE PD(II) AND ANTITUMOR CIS AMINE PT(II) COMPLEXES IN AQUEOUS-SOLUTIONS [J].

LIM, MC ;

MARTIN, RB .

JOURNAL OF INORGANIC & NUCLEAR CHEMISTRY, 1976, 38 (10) :1911-1914

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